熊取样胆酸颗粒项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号110755-202306对照品来源自制对照品使用方法直接使用
对照品含量(%)99.60对照品水分(%)0对照品稀释倍数200
标示量(mg)50供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.043706137125374483719236990371630.48
211.053669236698366950.02
单位质量响应值RSD%判断
3366.213320.810.97数据可信
加速2月-供试品溶液-25112801批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min120525-2052555.03056.252.5655.0356.252.56
220192-2019254.13754.14
321172-2117256.76556.76
421068-2106856.48656.49
521682-2168258.13258.13
621243-2124356.95556.96
10min130308-3030881.26080.611.6381.3580.701.63
229592-2959279.34079.43
329752-2975279.76979.86
430823-3082382.64182.73
530285-3028581.19881.30
629631-2963179.44579.54
15min135095-3509594.09492.691.1294.3292.921.12
234278-3427891.90492.13
334651-3465192.90493.13
434380-3438092.17792.41
534920-3492093.62593.86
634100-3410091.42791.65
20min136839-3683998.77095.772.0899.1596.162.07
235647-3564795.57495.95
336411-3641197.62398.01
435186-3518694.33894.72
535092-3509294.08694.47
635152-3515294.24794.63
30min136885-3688598.89497.351.3299.4497.901.32
236574-3657498.06098.59
336734-3673498.48999.03
436049-3604996.65297.19
535788-3578895.95296.50
635836-3583696.08196.62
45min136749-3674998.52996.162.1199.2496.862.10
236057-3605796.67497.37
336636-3663698.22698.94
434823-3482393.36594.07
535566-3556695.35796.06
635360-3536094.80595.50
60min136689-3668998.36896.931.7899.2597.801.77
236558-3655898.01798.88
336912-3691298.96699.84
435396-3539694.90195.76
535746-3574695.84096.70
635614-3561495.48696.34
极限136404-3640497.60496.171.6498.6597.201.63
235826-3582696.05497.08
335919-3591996.30497.34
434952-3495293.71194.73
536564-3656498.03399.06
635554-3555495.32596.34
熊取样胆酸颗粒项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号110755-202306对照品来源自制对照品使用方法直接使用
对照品含量(%)99.60对照品水分(%)0对照品稀释倍数200
标示量(mg)50供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.043721837393371233697437254371920.42
211.053704837453372500.77
单位质量响应值RSD%判断
3368.843371.040.05数据可信
加速2月-供试品溶液-25112801批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min121149-2114956.25657.663.6756.2657.663.67
221840-2184058.09458.09
321446-2144657.04657.05
420737-2073755.16055.16
523048-2304861.30761.31
621841-2184158.09758.10
10min131542-3154283.90182.351.9284.0082.441.92
231387-3138783.48983.59
330435-3043580.95781.05
430546-3054681.25281.34
531542-3154283.90184.00
630291-3029180.57480.67
15min134940-3494092.94092.431.1993.1792.661.19
234173-3417390.90091.14
335108-3510893.38793.62
434915-3491592.87393.10
535074-3507493.29693.54
634280-3428091.18491.42
20min136081-3608195.97597.302.7396.3697.682.72
236352-3635296.69697.08
336186-3618696.25496.64
436307-3630796.57696.96
535949-3594995.62496.02
638589-38589102.646103.03
30min135002-3500293.10596.092.5493.6596.642.52
236010-3601095.78696.33
336181-3618196.24196.79
437744-37744100.399100.94
536195-3619596.27896.84
635603-3560394.70495.26
45min135124-3512493.42996.621.9094.1397.341.89
236252-3625296.43097.14
336463-3646396.99197.70
436722-3672297.68098.39
536215-3621596.33197.05
637176-3717698.88899.60
60min136292-3629296.53696.170.7897.4097.040.77
236027-3602795.83196.70
336198-3619896.28697.15
436612-3661297.38798.26
535992-3599295.73896.62
635805-3580595.24196.12
极限136217-3621796.33795.960.9197.3696.990.91
235569-3556994.61395.64
335813-3581395.26296.29
436485-3648597.05098.09
536195-3619596.27897.32
636165-3616596.19897.23
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