褪黑素颗粒项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号520023-202203对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数10000
标示量(mg)1供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.956615965937660696582666051660080.20
29.956618366068661260.13
单位质量响应值RSD%判断
6633.976645.830.13数据可信
供试品溶液-2025041021批-水
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min169299-6929993.83794.410.7993.8494.410.79
270239-7023995.11095.11
370235-7023595.10495.10
469522-6952294.13994.14
570105-7010594.92894.93
668944-6894493.35693.36
10min169112-6911293.58494.501.3094.6395.551.30
269955-6995594.72595.78
370512-7051295.47996.54
468729-6872993.06594.11
571115-7111596.29697.35
669316-6931693.86094.90
15min169075-6907593.53493.931.1795.6296.031.16
270174-7017495.02297.13
370344-7034495.25297.37
468216-6821692.37094.45
569511-6951194.12496.25
668877-6887793.26695.35
20min168270-6827092.44492.330.7395.5795.470.74
268326-6832692.51995.68
368719-6871993.05296.23
467387-6738791.24894.35
568578-6857892.86196.03
667823-6782391.83894.95
30min166023-6602389.40189.930.9293.5594.100.92
266982-6698290.70094.89
366418-6641889.93694.15
465752-6575289.03493.15
567298-6729891.12795.33
666002-6600289.37393.51
极限165674-6567488.92889.241.2594.0794.411.22
266131-6613189.54794.75
366407-6640789.92195.13
464557-6455787.41692.53
566967-6696790.67995.89
665691-6569188.95194.08
褪黑素颗粒项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号520023-202203对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数10000
标示量(mg)1供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.956552165808656346568265599656490.17
29.956610866013660600.11
单位质量响应值RSD%判断
6597.896639.200.45数据可信
供试品溶液-AGP01批-水
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min171721-7172197.43197.850.6797.4397.850.67
272199-7219998.08098.08
371794-7179497.53097.53
472888-7288899.01699.02
571995-7199597.80397.80
671564-7156497.21897.22
10min171296-7129696.85397.351.4497.9498.441.42
271326-7132696.89497.98
371918-7191897.69898.78
472746-7274698.82399.92
570002-7000295.09696.18
672674-7267498.72599.81
15min169757-6975794.76395.951.3796.9298.121.34
271619-7161997.29299.46
369130-6913093.91196.08
471045-7104596.51298.71
571151-7115196.65698.80
671090-7109096.57498.75
20min170211-7021195.37996.080.5198.5999.320.50
270488-7048895.75699.00
371191-7119196.71199.92
470766-7076696.13399.40
570672-7067296.00699.22
671050-7105096.51999.77
30min167692-6769291.95894.031.2296.2398.331.19
269441-6944194.33398.64
369105-6910593.87798.16
470258-7025895.44399.78
569293-6929394.13298.42
669510-6951094.42798.75
极限168351-6835192.85393.480.8398.1598.830.82
269174-6917493.97199.33
368192-6819292.63797.97
469711-6971194.700100.10
568939-6893993.65298.98
668530-6853093.09698.47
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