布洛芬混悬液项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)0
对照品批号100179-202308对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数50
标示量(mg)200供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.962631570263706226361192633219263498826345920.09
211.022626490262933626279130.08
单位质量响应值RSD%判断
240382.48238467.600.57数据可信
加速3月-供试品溶液-2025103151批-pH7.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min12706902-2706902101.65299.412.74101.6599.412.74
22737809-2737809102.813102.81
32674956-2674956100.453100.45
42591232-259123297.30997.31
52626338-262633898.62798.63
62546293-254629395.62195.62
10min12712620-2712620101.86799.882.86102.43100.432.86
22763067-2763067103.762104.33
32700440-2700440101.410101.97
42603068-260306897.75398.29
52607023-260702397.90298.45
62572408-257240896.60297.13
15min12703237-2703237101.51599.243.02102.65100.353.02
22749001-2749001103.233104.38
32681008-2681008100.680101.80
42569205-256920596.48297.57
52601962-260196297.71298.80
62551856-255185695.83096.90
20min12665211-2665211100.08798.672.63101.78100.332.64
22732417-2732417102.611104.33
32657223-265722399.787101.47
42570257-257025796.52198.14
52587634-258763497.17498.81
62552229-255222995.84497.44
30min12667418-2667418100.17097.862.96102.42100.072.95
22717365-2717365102.045104.34
32618334-261833498.326100.56
42538985-253898595.34797.50
52576402-257640296.75298.93
62517209-251720994.52996.66
极限12550510-255051095.77995.180.7698.5997.930.76
22527261-252726194.90697.76
32523265-252326594.75697.54
42544924-254492495.57098.26
52555507-255550795.96798.68
62505413-250541394.08696.74
布洛芬混悬液项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)0
对照品批号100179-202308对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数50
标示量(mg)200供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.962630974263307626299262624745263145126300340.13
211.022629626262504426273350.13
单位质量响应值RSD%判断
239966.61238415.150.46数据可信
加速3月-供试品溶液-2025110151批-pH7.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min12607914-260791498.03095.951.4498.0395.951.44
22581826-258182697.05097.05
32528796-252879695.05695.06
42508125-250812594.27994.28
52537974-253797495.40195.40
62550584-255058495.87595.88
10min12616199-261619998.34295.791.8498.8996.321.84
22596483-259648397.60198.14
32527449-252744995.00695.53
42498017-249801793.90094.42
52521021-252102194.76495.29
62530878-253087895.13595.67
15min12600137-260013797.73895.271.7298.8396.341.72
22569258-256925896.57797.66
32488916-248891693.55794.61
42497053-249705393.86394.91
52513355-251335594.47695.53
62538139-253813995.40896.47
20min12605207-260520797.92995.062.0999.5696.662.09
22578149-257814996.91298.53
32477505-247750593.12894.70
42487576-248757693.50795.07
52492472-249247293.69195.27
62532721-253272195.20496.80
30min12547729-254772995.76894.481.3397.9596.601.34
22548172-254817295.78597.94
32490793-249079393.62895.72
42468704-246870492.79894.88
52494975-249497593.78595.89
62530537-253053795.12297.24
极限12550329-255032995.86694.421.7398.5897.061.71
22551467-255146795.90998.60
32482546-248254693.31895.93
42461866-246186692.54195.14
52550364-255036495.86798.49
62473786-247378692.98995.64
布洛芬混悬液项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)0
对照品批号100179-202308对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数50
标示量(mg)200供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.962627186263568126353522634778262882126323640.16
211.022634668263407426343710.02
单位质量响应值RSD%判断
240179.20239053.630.34数据可信
加速3月-供试品溶液-2025110251批-pH7.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min12548760-254876095.63695.720.8895.6495.720.88
22575513-257551396.64096.64
32544772-254477295.48795.49
42572487-257248796.52796.53
52513841-251384194.32694.33
62550769-255076995.71295.71
10min12576144-257614496.66496.660.4997.2097.190.49
22590071-259007197.18697.72
32571673-257167396.49697.03
42585259-258525997.00697.54
52553984-255398495.83296.36
62578951-257895196.76997.30
15min12547915-254791595.60595.550.6496.6796.620.65
22565148-256514896.25197.33
32545113-254511395.49996.57
42553507-255350795.81496.89
52516419-251641994.42395.48
62551161-255116195.72696.80
20min12545210-254521095.50395.570.6397.1097.170.62
22566638-256663896.30797.92
32564364-256436496.22297.82
42533351-253335195.05896.67
52527652-252765294.84496.43
62545099-254509995.49997.10
30min12540261-254026195.31795.070.9697.4597.200.95
22564860-256486096.24098.39
32538730-253873095.26097.39
42523832-252383294.70196.84
52492342-249234293.51995.63
62541466-254146695.36397.49
极限12504297-250429793.96894.280.7596.6396.940.74
22523216-252321694.67897.36
32529919-252991994.92997.59
42512589-251258994.27996.94
52479776-247977693.04895.68
62526376-252637694.79697.46
布洛芬混悬液项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)0
对照品批号100179-202308对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数50
标示量(mg)200供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.962631763263107726347622633630262860326319670.10
211.022631719262843626300780.09
单位质量响应值RSD%判断
240142.97238664.070.44数据可信
加速3月-供试品溶液-250226083批-pH7.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min12751925-2751925103.35299.382.18103.3599.382.18
22666545-2666545100.145100.15
32638734-263873499.10199.10
42607642-260764297.93397.93
52614791-261479198.20298.20
62597254-259725497.54397.54
10min12771750-2771750104.096100.921.68104.67101.481.68
22697296-2697296101.300101.86
32683645-2683645100.788101.34
42658457-265845799.842100.39
52662148-266214899.980100.53
62650208-265020899.532100.07
15min12760490-2760490103.674100.621.59104.83101.731.60
22686860-2686860100.908102.03
32671812-2671812100.343101.45
42646804-264680499.404100.50
52659257-265925799.872100.97
62649469-264946999.504100.60
20min12740644-2740644102.92899.951.65104.66101.621.65
22677254-2677254100.547102.23
32658861-265886199.857101.52
42627302-262730298.671100.32
52638600-263860099.096100.75
62625181-262518198.592100.24
30min12724054-2724054102.30599.481.55104.61101.711.56
22661113-266111399.941102.18
32647925-264792599.446101.67
42617286-261728698.295100.49
52626040-262604098.624100.83
62616494-261649498.266100.46
极限12715558-2715558101.98698.921.69104.85101.701.69
22652167-265216799.605102.40
32620819-262081998.428101.20
42601522-260152297.703100.45
52613480-261348098.152100.91
62599210-259921097.616100.36
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