布洛芬混悬液项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)0
对照品批号100179-202308对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数50
标示量(mg)200供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.962624944262532326213632630009262870826260690.13
211.022613867262341626186420.26
单位质量响应值RSD%判断
239604.84237626.320.59数据可信
中间条件3月-供试品溶液-2025103151批-pH7.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min12694683-2694683101.53799.181.79101.5499.181.79
22676251-2676251100.842100.84
32637367-263736799.37799.38
42571410-257141096.89296.89
52615291-261529198.54598.55
62597326-259732697.86997.87
10min12713508-2713508102.24699.871.62102.81100.421.62
22688359-2688359101.299101.86
32645886-264588699.698100.25
42602730-260273098.07298.61
52637416-263741699.37999.93
62614199-261419998.50499.05
15min12690614-2690614101.38499.221.61102.52100.331.61
22675251-2675251100.805101.93
32624844-262484498.905100.01
42583993-258399397.36698.45
52627552-262755299.007100.11
62596941-259694197.85498.95
20min12681826-2681826101.05398.961.37102.75100.611.37
22642286-264228699.563101.25
32629247-262924799.071100.73
42575332-257533297.04098.66
52622983-262298398.835100.48
62605493-260549398.17699.81
30min12661032-2661032100.26998.391.41102.53100.601.42
22639546-263954699.459101.70
32613035-261303598.460100.67
42563960-256396096.61198.77
52612638-261263898.446100.64
62576496-257649697.08499.26
极限12649044-264904499.81797.861.52102.63100.611.52
22628555-262855599.045101.83
32608223-260822398.279101.03
42551513-255151396.14298.84
52591499-259149997.649100.39
62554149-255414996.24298.96
布洛芬混悬液项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)0
对照品批号100179-202308对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数50
标示量(mg)200供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.962627072262561126243432633011262382126267720.15
211.022618614261918026188970.02
单位质量响应值RSD%判断
239668.98237649.460.60数据可信
中间条件3月-供试品溶液-2025110151批-pH7.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min12466874-246687492.93695.672.2692.9495.682.26
22629651-262965199.06999.07
32506471-250647194.42894.43
42577370-257737097.09997.10
52537718-253771895.60595.61
62519129-251912994.90594.90
10min12489609-248960993.79396.011.7794.3196.541.77
22616878-261687898.58799.14
32519535-251953594.92095.44
42580708-258070897.22597.76
52543290-254329095.81596.35
62540418-254041895.70796.23
15min12484578-248457893.60395.681.9594.6496.741.95
22625086-262508698.89799.99
32503975-250397594.33495.39
42561349-256134996.49597.57
52531805-253180595.38296.45
62530724-253072495.34296.40
20min12460370-246037092.69194.741.9894.2596.341.98
22602307-260230798.03899.69
32482064-248206493.50895.08
42522364-252236495.02796.64
52527835-252783595.23396.83
62493506-249350693.93995.53
30min12457182-245718292.57194.372.0894.6496.492.07
22586465-258646597.44299.63
32455053-245505392.49194.59
42541287-254128795.74097.88
52511343-251134394.61196.73
62477776-247777693.34795.46
极限12434963-243496391.73494.052.0194.3296.692.01
22582418-258241897.289100.02
32469835-246983593.04895.66
42516312-251631294.79997.47
52493253-249325393.93096.58
62481128-248112893.47396.10
布洛芬混悬液项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)0
对照品批号100179-202308对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数50
标示量(mg)200供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.962619436262440126264332625135262470626240220.11
211.022621103262352526223140.07
单位质量响应值RSD%判断
239418.07237959.530.44数据可信
中间条件3月-供试品溶液-2025110251批-pH7.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min12661645-2661645100.26198.081.39100.2698.081.39
22600541-260054197.95997.96
32601966-260196698.01398.01
42622190-262219098.77498.77
52557018-255701896.31996.32
62579414-257941497.16397.16
10min12670271-2670271100.58598.131.61101.1498.671.60
22567965-256796596.73297.28
32631053-263105399.10899.65
42617269-261726998.58999.14
52571536-257153696.86697.40
62571720-257172096.87397.41
15min12658336-2658336100.13697.911.65101.2599.001.64
22576005-257600597.03598.12
32624027-262402798.84499.94
42624633-262463398.86699.96
52551223-255122396.10197.17
62560574-256057496.45397.53
20min12624013-262401398.84397.241.34100.5298.871.34
22594003-259400397.71399.33
32590051-259005197.56499.21
42599871-259987197.93499.58
52549665-254966596.04297.65
62530604-253060495.32496.94
30min12622379-262237998.78196.741.65101.0098.911.64
22569202-256920296.77898.94
32579512-257951297.16799.35
42599901-259990197.935100.12
52516400-251640094.78996.93
62521255-252125594.97297.12
极限12612696-261269698.41796.351.50101.1999.061.50
22548136-254813695.98598.69
32570634-257063496.83299.56
42579089-257908997.15199.88
52503113-250311394.28996.96
62532602-253260295.40098.07
布洛芬混悬液项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)0
对照品批号100179-202308对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数50
标示量(mg)200供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.962621712262353526276192627376262316126246810.11
211.022624632262192726232800.08
单位质量响应值RSD%判断
239478.19238047.190.43数据可信
中间条件3月-供试品溶液-250226083批-pH7.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min12633214-263321499.15998.891.1599.1698.891.15
22635449-263544999.24399.24
32678217-2678217100.854100.85
42606130-260613098.13998.14
52595550-259555097.74197.74
62608385-260838598.22498.22
10min12668249-2668249100.478100.450.64101.03101.000.65
22667944-2667944100.467101.02
32697679-2697679101.586102.15
42647556-264755699.699100.24
52655701-2655701100.006100.55
62667965-2667965100.467101.01
15min12702947-2702947101.785100.310.89102.89101.420.89
22657785-2657785100.084101.19
32682395-2682395101.011102.14
42645603-264560399.625100.72
52649454-264945499.770100.87
62645263-264526399.613100.72
20min12628892-262889298.99699.390.58100.67101.050.58
22646439-264643999.657101.32
32666877-2666877100.427102.11
42628586-262858698.985100.64
52629543-262954399.021100.67
62635128-263512899.231100.89
30min12617344-261734498.56198.790.61100.79101.000.61
22631757-263175799.104101.32
32651181-265118199.835102.08
42620652-262065298.686100.89
52609413-260941398.263100.47
62609592-260959298.269100.48
极限12609488-260948898.26598.280.53101.04101.040.53
22611605-261160598.345101.11
32631359-263135999.089101.89
42615504-261550498.492101.24
52598909-259890997.867100.62
62592150-259215097.613100.37
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