褪黑素颗粒项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号520023-202203对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数10000
标示量(mg)1供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.956617866062658526586765875659670.23
29.956615266126661390.03
单位质量响应值RSD%判断
6629.856647.140.19数据可信
供试品溶液-2025041021批-水
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min169870-6987094.63091.265.1394.6391.265.14
270894-7089496.01796.02
370273-7027395.17695.18
465898-6589889.25189.25
562438-6243884.56584.56
664901-6490187.90087.90
10min169482-6948294.10593.181.4995.1694.201.45
269047-6904793.51694.58
366923-6692390.63991.70
468732-6873293.08994.08
569870-6987094.63095.57
668754-6875493.11994.10
15min169493-6949394.12093.340.9596.2295.380.96
269809-6980994.54896.65
368149-6814992.29994.36
468694-6869493.03895.06
568331-6833192.54694.54
669012-6901293.46895.48
20min168041-6804192.15393.051.3295.3096.141.26
268869-6886993.27596.43
367625-6762591.59094.68
469922-6992294.70197.76
568214-6821492.38795.41
669560-6956094.21097.26
30min167437-6743791.33591.991.0595.5096.111.02
268687-6868793.02897.22
367050-6705090.81194.92
468665-6866592.99897.11
567412-6741291.30195.35
668266-6826692.45896.55
极限166383-6638389.90890.670.7395.0995.810.70
267160-6716090.96096.19
366673-6667390.30095.42
467181-6718190.98896.13
566572-6657290.16495.22
667689-6768991.67696.80
褪黑素颗粒项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号520023-202203对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数10000
标示量(mg)1供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.956687367269670016681866743669410.31
29.956633866017661780.35
单位质量响应值RSD%判断
6727.746651.060.82数据可信
供试品溶液-2025041021批-水
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min169786-6978693.80093.041.5693.8093.041.56
270025-7002594.12194.12
370176-7017694.32494.32
468345-6834591.86391.86
569528-6952893.45393.45
667472-6747290.69090.69
10min168724-6872492.37392.640.5793.4193.670.55
268633-6863392.25093.30
368434-6843491.98393.03
469182-6918292.98894.01
569460-6946093.36294.40
669095-6909592.87193.88
15min168864-6886492.56192.170.6994.6394.230.67
268720-6872092.36794.44
368662-6866292.28994.36
467649-6764990.92892.98
568613-6861392.22494.30
668924-6892492.64294.68
20min166898-6689889.91890.321.1193.0293.401.07
266314-6631489.13392.23
367350-6735090.52693.62
467990-6799091.38694.45
568083-6808391.51194.61
666535-6653589.43092.50
30min167891-6789191.25390.430.9595.3594.520.92
266175-6617588.94793.03
367798-6779891.12895.23
467043-6704390.11394.19
567157-6715790.26694.38
667607-6760790.87194.93
极限166422-6642289.27989.770.5694.3994.870.54
266497-6649789.37994.46
367226-6722690.35995.47
466800-6680089.78794.87
567250-6725090.39195.51
666534-6653489.42994.50
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