达格列净片项目信息
介质体积(ml)1000取样体积(ml)1.5补液体积(ml)1.5
对照品批号101568-202301对照品来源中检院对照品使用方法直接使用
对照品含量(%)80.4对照品水分(%)0对照品稀释倍数1000
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
1 12.121991861996271994031995161995501994560.09
2 12.202002732000142001440.10
单位质量响应值RSD%判断
16456.7716405.250.23数据可信
加速6月-供试品溶液-2025080321批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1172985-17298584.64585.040.9384.6585.040.93
2173768-17376885.02885.03
3172498-17249884.40784.41
4175945-17594586.09386.09
5172067-17206784.19684.20
6175514-17551485.88385.88
10min1184809-18480990.43191.361.1090.5691.481.10
2185430-18543090.73590.86
3184550-18455090.30490.43
4189558-18955892.75592.88
5187887-18788791.93792.06
6187984-18798491.98492.11
15min1190614-19061493.27194.251.2193.5394.521.21
2191716-19171693.81094.07
3190244-19024493.09093.35
4196533-19653396.16896.44
5193650-19365094.75795.02
6192943-19294394.41194.68
20min1193525-19352594.69695.901.2595.1096.311.25
2194909-19490995.37395.78
3193957-19395794.90795.31
4200184-20018497.95498.37
5196732-19673296.26596.67
6196664-19666496.23296.64
30min1197260-19726096.52397.661.4097.0798.211.39
2197719-19771996.74897.30
3196810-19681096.30396.85
4203659-20365999.654100.21
5201839-20183998.76499.31
6200219-20021997.97198.52
45min1197848-19784896.81198.481.4797.5099.181.47
2200434-20043498.07698.77
3198151-19815196.95997.65
4205258-205258100.437101.15
5202945-20294599.305100.00
6202961-20296199.313100.01
极限1197891-19789196.83298.391.7297.6799.241.71
2198959-19895997.35598.19
3197302-19730296.54497.38
4205435-205435100.523101.38
5203181-20318199.421100.27
6203740-20374099.694100.54
达格列净片项目信息
介质体积(ml)1000取样体积(ml)1.5补液体积(ml)1.5
对照品批号101568-202301对照品来源中检院对照品使用方法直接使用
对照品含量(%)80.4对照品水分(%)0对照品稀释倍数1000
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
1 12.122006262003372005482004282007522005380.09
2 12.201998041998871998460.03
单位质量响应值RSD%判断
16546.0416380.820.71数据可信
加速6月-供试品溶液-2025080421批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1176362-17636286.12985.900.8186.1385.900.81
2175890-17589085.89985.90
3177308-17730886.59186.59
4174790-17479085.36285.36
5177248-17724886.56286.56
6173703-17370384.83184.83
10min1188307-18830791.96392.311.1192.0992.441.11
2192829-19282994.17194.30
3189809-18980992.69792.83
4187918-18791891.77391.90
5188411-18841192.01492.14
6186852-18685291.25291.38
15min1194039-19403994.76294.870.7395.0395.130.73
2195055-19505595.25995.53
3196558-19655895.99396.26
4193947-19394794.71794.98
5193478-19347894.48894.76
6192438-19243893.98094.24
20min1197620-19762096.51196.590.7596.9297.000.75
2198088-19808896.74097.15
3200415-20041597.87698.29
4197655-19765596.52896.94
5196660-19666096.04296.45
6196223-19622395.82996.23
30min1200398-20039897.86898.161.2098.4298.711.20
2201942-20194298.62299.18
3205065-205065100.147100.71
4200943-20094398.13498.69
5197982-19798296.68897.24
6199632-19963297.49498.04
45min1201810-20181098.55798.911.3399.2699.611.32
2203004-20300499.14199.85
3207674-207674101.421102.13
4201437-20143798.37599.08
5200513-20051397.92498.62
6200720-20072098.02598.72
极限1201395-20139598.35598.871.8399.2099.721.82
2203277-20327799.274100.13
3209169-209169102.151103.01
4202005-20200598.65399.50
5200730-20073098.03098.88
6198174-19817496.78297.62
达格列净片项目信息
介质体积(ml)1000取样体积(ml)1.5补液体积(ml)1.5
对照品批号101568-202301对照品来源中检院对照品使用方法直接使用
对照品含量(%)80.4对照品水分(%)0对照品稀释倍数1000
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
1 12.121991771992641993361994681996041993700.09
2 12.201992411988911990660.13
单位质量响应值RSD%判断
16449.6716316.890.58数据可信
加速6月-供试品溶液-2025080521批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1172440-17244084.62585.230.8584.6385.230.85
2174656-17465685.71385.71
3175684-17568486.21786.22
4173520-17352085.15585.16
5174087-17408785.43485.43
6171633-17163384.22984.23
10min1185023-18502390.80091.141.1090.9391.271.10
2187521-18752192.02692.15
3188099-18809992.31092.44
4185417-18541790.99491.12
5185874-18587491.21891.35
6182378-18237889.50289.63
15min1190843-19084393.65793.601.2493.9293.871.24
2192572-19257294.50594.77
3193181-19318194.80495.07
4190162-19016293.32293.59
5191138-19113893.80194.07
6186513-18651391.53291.79
20min1194123-19412395.26694.861.3395.6795.261.33
2195939-19593996.15896.57
3195504-19550495.94496.35
4191962-19196294.20694.61
5193196-19319694.81195.22
6188999-18899992.75293.15
30min1197056-19705696.70696.111.3097.2596.661.30
2198452-19845297.39197.94
3197578-19757896.96297.52
4194471-19447195.43795.98
5196071-19607196.22296.77
6191465-19146593.96294.50
45min1199407-19940797.85996.731.3298.5597.421.31
2198607-19860797.46798.17
3198664-19866497.49598.19
4196078-19607896.22696.91
5197529-19752996.93897.63
6192400-19240094.42195.10
极限1199487-19948797.89996.621.3398.7497.451.33
2198552-19855297.44098.28
3197998-19799897.16898.01
4195059-19505995.72696.56
5197665-19766597.00597.84
6192485-19248594.46295.28
达格列净片项目信息
介质体积(ml)1000取样体积(ml)1.5补液体积(ml)1.5
对照品批号101568-202301对照品来源中检院对照品使用方法直接使用
对照品含量(%)80.4对照品水分(%)0对照品稀释倍数1000
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
1 12.122001392007272006512007982003292005290.15
2 12.202033962018842026400.53
单位质量响应值RSD%判断
16545.3016609.840.28数据可信
加速6月-供试品溶液-WK2927批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1175483-17548385.10884.564.1985.1184.564.19
2164101-16410179.58879.59
3179237-17923786.92986.93
4180745-18074587.66087.66
5166467-16646780.73680.74
6180101-18010187.34887.35
10min1194149-19414994.16194.610.9994.2994.740.99
2194393-19439394.28094.40
3194856-19485694.50494.63
4192915-19291593.56393.69
5198552-19855296.29796.42
6195632-19563294.88095.01
15min1196968-19696895.52895.631.1495.8095.901.13
2196792-19679295.44395.70
3197315-19731595.69795.97
4194229-19422994.20094.47
5201136-20113697.55097.82
6196651-19665195.37595.65
20min1197335-19733595.70695.681.1796.1296.101.17
2197128-19712895.60696.01
3197117-19711795.60196.02
4194222-19422294.19794.61
5201364-20136497.66098.07
6196550-19655095.32695.74
30min1197431-19743195.75395.931.1896.3196.491.17
2197528-19752895.80096.35
3197299-19729995.68996.25
4195085-19508594.61595.17
5202148-20214898.04198.60
6197288-19728895.68496.24
45min1196853-19685395.47395.691.4096.1796.391.39
2196576-19657695.33896.03
3196626-19662695.36396.07
4194107-19410794.14194.84
5202426-20242698.17698.88
6197218-19721895.65096.35
极限1196135-19613595.12495.251.4395.9796.101.43
2195904-19590495.01295.85
3196603-19660395.35196.20
4193910-19391094.04594.88
5201666-20166697.80798.66
6194159-19415994.16695.01
点击查看处理图标(人工保存)
　
原始图谱下载图谱(姜进硙 于 2026-03-12 13:26:50 完成)
生成报告数据部分(等待生成报告)
Current page cost:59 ms