诺氟沙星胶囊项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号130450-201907对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.6对照品水分(%)0对照品稀释倍数100
标示量(mg)100 供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.983958019394732539468313943244395048739491810.15
210.104000386400610940032480.11
单位质量响应值RSD%判断
395709.52396361.190.12数据可信
供试品溶液-24042301批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min14196437-419643794.98489.584.2894.9889.584.28
24077438-407743892.29092.29
33872254-387225487.64687.65
43709328-370932883.95883.96
53982757-398275790.14790.15
63909219-390921988.48388.48
10min14462810-4462810101.01399.552.01101.1799.702.00
24316950-431695097.71197.87
34351495-435149598.49398.64
44449880-4449880100.720100.86
54296692-429669297.25397.40
64511888-4511888102.124102.27
15min14456036-4456036100.86099.641.90101.1999.961.89
24353352-435335298.53598.85
34364380-436438098.78599.10
44440563-4440563100.509100.82
54284107-428410796.96897.28
64514236-4514236102.177102.49
20min14459134-4459134100.93099.611.92101.42100.101.91
24342901-434290198.29998.78
34350929-435092998.48098.96
44444253-4444253100.593101.07
54294094-429409497.19497.67
64514618-4514618102.185102.67
30min14444975-4444975100.60999.761.78101.27100.411.78
24343892-434389298.32198.97
34366733-436673398.83899.48
44449619-4449619100.714101.36
54315865-431586597.68798.32
64523416-4523416102.385103.04
诺氟沙星胶囊项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号130450-201907对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.6对照品水分(%)0对照品稀释倍数100
标示量(mg)100 供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.983997258399384239949983999274399439439959530.06
210.103975554397314039743470.05
单位质量响应值RSD%判断
400396.09393499.701.23数据可信
供试品溶液-24042301批-pH4.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min12612520-261252059.00158.7512.2959.0058.7412.28
22931021-293102166.19466.19
32326861-232686152.55052.55
42991201-299120167.55367.55
52186099-218609949.37149.37
62559880-255988057.81257.81
10min13786147-378614785.50683.635.3485.6083.735.34
23994499-399449990.21290.32
33685548-368554883.23483.32
43635487-363548782.10482.22
53390577-339057776.57376.66
63726011-372601184.14884.24
15min14257946-425794696.16293.602.6096.4093.842.60
24271925-427192596.47796.74
34177979-417797994.35694.58
44032395-403239591.06891.32
54032391-403239191.06891.28
64095126-409512692.48492.72
20min14304654-430465497.21695.491.9597.6295.881.95
24335222-433522297.90798.33
34250005-425000595.98296.37
44128597-412859793.24093.64
54159708-415970893.94394.30
64191383-419138394.65895.05
30min14328947-432894797.76595.561.9098.3396.121.90
24313359-431335997.41398.00
34259531-425953196.19796.74
44142571-414257193.55694.11
54177051-417705194.33594.85
64167048-416704894.10994.66
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