普瑞巴林口崩片项目信息
介质体积(ml)900取样体积(ml)0补液体积(ml)0
对照品批号101106-202003对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.4对照品水分(%)0对照品稀释倍数100
标示量(mg)150供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
116.991062111058821061941056161059251059660.24
217.081053791055101054440.09
单位质量响应值RSD%判断
6236.966173.540.73数据可信
供试品溶液-LW0477批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
2min159908-5990857.58055.412.9657.5855.412.96
255173-5517353.02953.03
358595-5859556.31856.32
457679-5767955.43855.44
556245-5624554.06054.06
658290-5829056.02556.03
5min197008-9700893.23992.760.7793.2492.760.77
297585-9758593.79493.79
396241-9624192.50292.50
496564-9656492.81292.81
595407-9540791.70091.70
696282-9628292.54192.54
10min1102247-10224798.27498.500.9398.2798.500.93
2103899-10389999.86299.86
3102173-10217398.20398.20
4103368-10336899.35299.35
5101782-10178297.82797.83
6101432-10143297.49197.49
15min1102623-10262398.63699.141.2998.6499.151.29
2104529-104529100.468100.47
3104287-104287100.235100.24
4104098-104098100.053100.05
5101967-10196798.00598.01
6101411-10141197.47197.47
30min1102624-10262498.63799.160.8098.6499.160.80
2104051-104051100.008100.01
3103763-10376399.73199.73
4103843-10384399.80899.81
5102072-10207298.10698.11
6102657-10265798.66898.67
普瑞巴林口崩片项目信息
介质体积(ml)900取样体积(ml)0补液体积(ml)0
对照品批号101106-202003对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.4对照品水分(%)0对照品稀释倍数100
标示量(mg)150供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
116.991054641056461055711054631052901054870.13
217.081049481050091049780.05
单位质量响应值RSD%判断
6208.776146.250.72数据可信
供试品溶液-LW0477批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
2min161745-6174559.61258.821.3959.6158.821.39
261654-6165459.52559.52
361404-6140459.28359.28
460756-6075658.65858.66
560454-6045458.36658.37
659552-5955257.49557.50
5min197557-9755794.18895.410.8494.1995.400.84
298838-9883895.42495.42
399774-9977496.32896.33
499313-9931395.88395.88
599292-9929295.86395.86
698134-9813494.74594.74
10min1102838-10283899.286100.801.4099.29100.801.40
2104948-104948101.323101.32
3106410-106410102.735102.73
4104401-104401100.795100.80
5105202-105202101.569101.57
6102609-10260999.06599.07
15min1102860-10286099.307100.681.4599.31100.681.45
2104780-104780101.161101.16
3106809-106809103.120103.12
4104019-104019100.426100.43
5104544-104544100.933100.93
6102670-10267099.12499.12
30min1102745-10274599.196100.601.3299.20100.601.32
2104521-104521100.911100.91
3106384-106384102.710102.71
4104058-104058100.464100.46
5104709-104709101.093101.09
6102753-10275399.20499.20
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