布洛芬混悬液项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)0
对照品批号100179-202308对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数50
标示量(mg)200供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
1 11.032645284266070826561272647658265169326522940.24
2 10.942644466264567226450690.04
单位质量响应值RSD%判断
240461.83241779.620.39数据可信
中间条件6月-供试品溶液-2025103151批-pH7.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min12636912-263691298.32797.611.3198.3397.611.31
22658379-265837999.12799.13
32628639-262863998.01898.02
42625946-262594697.91897.92
52562064-256206495.53695.54
62594145-259414596.73296.73
10min12658216-265821699.12198.171.1899.6798.721.18
22647579-264757998.72599.28
32660644-266064499.21299.76
42642220-264222098.52599.07
52592803-259280396.68297.21
62595066-259506696.76797.30
15min12629541-262954198.05297.491.1299.1598.581.12
22643385-264338598.56899.67
32638065-263806598.37099.47
42619452-261945297.67698.77
52578801-257880196.16097.23
62577784-257778496.12297.20
20min12633612-263361298.20497.011.2799.8598.641.27
22620642-262064297.72099.37
32622001-262200197.77199.41
42608397-260839797.26498.90
52547109-254710994.97896.58
62577077-257707796.09697.70
30min12613650-261365097.45996.701.2499.6598.861.24
22618718-261871897.64899.84
32612192-261219297.40599.59
42610845-261084597.35599.53
52553409-255340995.21397.34
62550272-255027295.09697.24
极限12603307-260330797.07496.261.0799.8098.961.07
22599071-259907196.91699.65
32603407-260340797.07899.80
42589920-258992096.57599.29
52545357-254535794.91397.57
62547685-254768595.00097.67
布洛芬混悬液项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)0
对照品批号100179-202308对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数50
标示量(mg)200供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
1 11.032647010264822026499242654429264920826497580.11
2 10.942641903264242726421650.02
单位质量响应值RSD%判断
240231.91241514.170.38数据可信
中间条件6月-供试品溶液-2025110151批-pH7.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min12524228-252422894.22295.600.9494.2295.600.94
22597201-259720196.94696.95
32571678-257167895.99395.99
42564314-256431495.71895.72
52554266-255426695.34395.34
62555263-255526395.38095.38
10min12524626-252462694.23796.411.2594.7696.941.25
22619787-261978797.78998.33
32585857-258585796.52297.06
42599998-259999897.05097.58
52591048-259104896.71697.25
62575649-257564996.14196.67
15min12517475-251747593.97095.871.0595.0296.941.05
22587071-258707196.56897.65
32586265-258626596.53797.61
42584470-258447096.47097.54
52573613-257361396.06597.13
62561286-256128695.60596.67
20min12501884-250188493.38895.401.1794.9697.001.17
22580931-258093196.33897.96
32569684-256968495.91997.52
42580728-258072896.33197.94
52554555-255455595.35496.95
62547145-254714595.07796.67
30min12485934-248593492.79294.811.1294.8896.941.12
22564487-256448795.72597.88
32548449-254844995.12697.26
42558193-255819395.49097.63
52547366-254736695.08597.22
62535919-253591994.65896.78
极限12459758-245975891.81594.161.3194.4296.821.30
22553320-255332095.30897.99
32530465-253046594.45597.12
42537644-253764494.72397.40
52517510-251751093.97196.63
62537431-253743194.71597.36
布洛芬混悬液项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)0
对照品批号100179-202308对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数50
标示量(mg)200供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
1 11.032641888264647826379882638307264240926414140.14
2 10.942649030263863126438300.28
单位质量响应值RSD%判断
239475.43241666.360.65数据可信
中间条件6月-供试品溶液-2025110251批-pH7.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min12597027-259702797.06295.301.5197.0695.301.51
22586441-258644196.66796.67
32560533-256053395.69895.70
42538722-253872294.88394.88
52516687-251668794.06094.06
62499799-249979993.42893.43
10min12594286-259428696.96096.291.0797.5096.821.07
22613278-261327897.67098.21
32584953-258495396.61197.14
42575631-257563196.26396.79
52549699-254969995.29395.82
62540728-254072894.95895.48
15min12574845-257484596.23395.650.9797.3196.710.97
22574729-257472996.22997.31
32593063-259306396.91497.98
42541010-254101094.96996.03
52536842-253684294.81395.86
62535086-253508694.74795.79
20min12580294-258029496.43795.330.9998.0596.931.00
22569025-256902596.01697.63
32560293-256029395.68997.30
42550796-255079695.33496.92
52510842-251084293.84195.42
62533593-253359394.69196.26
30min12544273-254427395.09194.631.1097.2496.761.09
22552531-255253195.39997.55
32569062-256906296.01798.16
42496403-249640393.30195.42
52517543-251754394.09296.19
62512333-251233393.89796.00
极限12550045-255004595.30694.190.9597.9896.840.95
22529476-252947694.53897.22
32537369-253736994.83397.50
42516853-251685394.06696.70
52484731-248473192.86595.49
62502528-250252893.53096.15
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