布洛芬混悬液项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)0
对照品批号100179-202308对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数50
标示量(mg)200供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.032641319264982026506362649335264744526477110.15
2 10.942655267264793126515990.20
单位质量响应值RSD%判断
240046.33242376.510.69数据可信
长期6月-供试品溶液-2025103151批-pH7.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min12637555-263755598.31597.991.3598.3298.001.35
22660516-266051699.17199.17
32673431-267343199.65399.65
42621927-262192797.73397.73
52580958-258095896.20696.21
62599234-259923496.88796.89
10min12640147-264014798.41298.001.4998.9698.551.48
22666098-266609899.37999.93
32671228-267122899.571100.12
42620948-262094897.69698.24
52609836-260983697.28297.82
62566780-256678095.67796.22
15min12631559-263155998.09297.441.7099.1898.521.69
22665465-266546599.356100.46
32646995-264699598.66799.77
42611394-261139497.34098.43
52583898-258389896.31597.39
62544378-254437894.84295.91
20min12614543-261454397.45896.931.4199.1098.561.41
22648620-264862098.728100.38
32627787-262778797.95199.61
42583528-258352896.30297.93
52578965-257896596.13197.74
62548882-254888295.01096.61
30min12603189-260318997.03496.231.7699.2198.401.76
22628152-262815297.965100.17
32624370-262437097.824100.02
42565632-256563295.63597.80
52557813-255781395.34397.49
62510631-251063193.58495.71
极限12584914-258491496.35395.731.3799.0798.431.37
22607262-260726297.18699.93
32596142-259614296.77299.51
42562728-256272895.52698.22
52543535-254353594.81197.48
62514055-251405593.71296.36
布洛芬混悬液项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)0
对照品批号100179-202308对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数50
标示量(mg)200供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.032648725264596826532502652670265076226502750.12
2 10.942643732263969326417120.11
单位质量响应值RSD%判断
240278.79241472.760.36数据可信
长期6月-供试品溶液-2025110151批-pH7.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min12567998-256799895.85495.231.5595.8595.231.55
22611624-261162497.48397.48
32568443-256844395.87195.87
42541024-254102494.84894.85
52508100-250810093.61993.62
62511023-251102393.72893.73
10min12599302-259930297.02395.941.3097.5696.471.30
22614723-261472397.59998.14
32561717-256171795.62096.15
42575811-257581196.14696.67
52525836-252583694.28194.80
62544735-254473594.98695.51
15min12567420-256742095.83395.211.3896.9096.271.38
22599804-259980497.04298.13
32567732-256773295.84596.91
42543838-254383894.95396.01
52521556-252155694.12195.16
62503454-250345493.44594.49
20min12564982-256498295.74294.911.3497.3596.501.34
22586841-258684196.55898.18
32562686-256268695.65697.25
42527640-252764094.34895.94
52497765-249776593.23394.80
62516401-251640193.92995.50
30min12532861-253286194.54394.161.4596.6896.281.45
22571679-257167995.99298.15
32548349-254834995.12197.25
42519823-251982394.05696.17
52487999-248799992.86894.95
62474649-247464992.37094.46
极限12524930-252493094.24793.761.0296.9196.411.03
22549211-254921195.15397.85
32521274-252127494.11096.77
42508449-250844993.63296.27
52480766-248076692.59895.20
62487397-248739792.84695.45
布洛芬混悬液项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)0
对照品批号100179-202308对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数50
标示量(mg)200供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.032641550264554126508972643644264717026457600.14
2 10.942650297264607026481840.12
单位质量响应值RSD%判断
239869.45242064.350.65数据可信
长期6月-供试品溶液-2025110251批-pH7.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min12637945-263794598.43095.852.1898.4395.862.18
22621234-262123497.80697.81
32575797-257579796.11196.11
42557486-255748695.42795.43
52533606-253360694.53694.54
62487228-248722892.80692.81
10min12644252-264425298.66596.271.9999.2196.801.99
22631714-263171498.19798.74
32576892-257689296.15196.69
42575979-257597996.11796.65
52539171-253917194.74495.27
62512187-251218793.73794.25
15min12634460-263446098.29996.011.9199.3997.081.91
22621230-262123097.80698.89
32575833-257583396.11297.18
42565839-256583995.73996.80
52534588-253458894.57395.62
62506855-250685593.53894.57
20min12617316-261731697.66095.412.0899.3097.012.08
22613962-261396297.53599.17
32562047-256204795.59897.20
42549779-254977995.14096.74
52514734-251473493.83295.41
62484138-248413892.69194.25
30min12600566-260056697.03594.941.9199.2297.071.91
22586171-258617196.49898.67
32556815-255681595.40297.54
42539437-253943794.75496.88
52515663-251566393.86795.97
62467684-246768492.07794.15
极限12589131-258913196.60894.361.9199.3397.021.91
22573571-257357196.02898.74
32542642-254264294.87397.54
42513114-251311493.77296.42
52488656-248865692.85995.48
62466135-246613592.01994.60
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