辅酶Q10片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号140611-202107对照品来源中检所对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数500
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.052684332698822691882703812703152696400.31
210.072713192716592714890.09
单位质量响应值RSD%判断
26829.8526960.180.35数据可信
供试品溶液-24123001批-pH2.0盐酸溶液
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1210647-21064778.16676.012.7778.1776.012.78
2207580-20758077.02877.03
3208346-20834677.31277.31
4204177-20417775.76575.76
5203658-20365875.57275.57
6194580-19458072.20472.20
10min1222402-22240282.52882.221.5882.7682.451.59
2223328-22332882.87183.10
3224956-22495683.47583.71
4220593-22059381.85682.08
5223125-22312582.79683.02
6215043-21504379.79780.01
15min1227028-22702884.24484.051.3984.7384.531.39
2228545-22854584.80785.29
3229201-22920185.05185.53
4225079-22507983.52183.99
5228359-22835984.73885.21
6220872-22087281.96082.42
20min1227457-22745784.40484.751.0685.1485.481.06
2229624-22962485.20885.94
3231181-23118185.78586.52
4226424-22642484.02084.74
5230522-23052285.54186.27
6225161-22516183.55284.25
30min1227963-22796384.59185.441.2385.5886.421.23
2232574-23257486.30287.29
3233052-23305286.48087.47
4228793-22879384.89985.87
5232555-23255586.29587.28
6226493-22649384.04685.00
45min1229673-22967385.22686.091.0286.4787.331.02
2232744-23274486.36587.61
3234812-23481287.13388.39
4229942-22994285.32686.56
5234610-23461087.05888.30
6230288-23028885.45486.66
60min1230855-23085585.66486.820.9287.1688.310.92
2235339-23533987.32888.84
3234992-23499287.20088.72
4232235-23223586.17787.66
5236637-23663787.81089.32
6233684-23368486.71488.18
极限1251146-25114693.19494.471.0294.9596.231.02
2257636-25763695.60297.37
3255612-25561294.85196.63
4252140-25214093.56395.31
5256894-25689495.32797.10
6254144-25414494.30696.03
辅酶Q10片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号140611-202107对照品来源中检所对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数500
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.052707072703802703942709292708762706570.10
210.072713072715742714400.07
单位质量响应值RSD%判断
26931.0426955.310.07数据可信
供试品溶液-24123002批
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1216039-21603980.02379.392.2380.0279.392.24
2222634-22263482.46682.47
3212394-21239478.67378.67
4208295-20829577.15477.15
5213056-21305678.91878.92
6213623-21362379.12879.13
10min1230927-23092785.53785.801.9885.7886.041.98
2238557-23855788.36488.61
3229273-22927384.92585.16
4225606-22560683.56783.80
5235157-23515787.10487.34
6230353-23035385.32585.56
15min1235111-23511187.08787.421.8187.5887.921.82
2244042-24404290.39590.91
3234336-23433686.80087.29
4231385-23138585.70786.19
5236434-23643487.57788.08
6234810-23481086.97687.47
20min1235787-23578787.33888.151.9688.1088.911.96
2247077-24707791.52092.30
3236671-23667187.66588.42
4234017-23401786.68287.42
5238126-23812688.20488.96
6236213-23621387.49588.25
30min1236892-23689287.74788.611.8288.7789.631.82
2247113-24711391.53392.59
3237771-23777188.07389.09
4234339-23433986.80187.80
5239893-23989388.85989.88
6239280-23928088.63289.65
45min1239917-23991788.86789.211.8090.1590.501.80
2248973-24897392.22293.55
3239764-23976488.81190.09
4235881-23588187.37288.63
5240064-24006488.92290.21
6240446-24044689.06390.35
60min1239857-23985788.84589.301.7990.4090.861.80
2249430-24943092.39194.00
3240003-24000388.89990.44
4236746-23674687.69389.21
5240749-24074989.17690.73
6239792-23979288.82190.37
极限1262884-26288497.37596.361.4699.1998.181.46
2263263-26326397.51599.40
3258363-25836395.70097.51
4253660-25366093.95895.74
5263157-26315797.47699.30
6259601-25960196.15997.97
辅酶Q10片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号140611-202107对照品来源中检所对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数500
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.052719142725022722652719392714352720110.15
210.072715042722512718780.20
单位质量响应值RSD%判断
27065.7726998.810.18数据可信
供试品溶液-24123003批
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1166120-16612061.33058.044.1361.3358.044.13
2163526-16352660.37260.37
3157357-15735758.09458.09
4154860-15486057.17357.17
5151162-15116255.80755.81
6150200-15020055.45255.45
10min1193521-19352171.44668.482.4571.6368.652.45
2187943-18794369.38669.57
3184404-18440468.08068.25
4182776-18277667.47967.65
5182900-18290067.52567.69
6181388-18138866.96667.13
15min1204190-20419075.38573.011.7175.7873.391.71
2196611-19661172.58772.98
3196877-19687772.68573.06
4195314-19531472.10872.48
5198402-19840273.24873.62
6195150-19515072.04772.41
20min1210331-21033177.65275.861.4178.2876.461.41
2203654-20365475.18775.79
3204240-20424075.40376.00
4202870-20287074.89775.49
5207636-20763676.65777.25
6204127-20412775.36175.94
30min1219425-21942581.00979.411.5481.8780.231.54
2210856-21085677.84678.68
3213645-21364578.87579.70
4214864-21486479.32580.14
5218556-21855680.68881.51
6213140-21314078.68979.50
45min1225237-22523783.15581.971.6584.2683.041.64
2218535-21853580.68181.75
3219404-21940481.00182.06
4221622-22162281.82082.87
5227686-22768684.05985.12
6219680-21968081.10382.15
60min1227026-22702683.81583.361.7185.1784.681.69
2222209-22220982.03783.35
3222712-22271282.22383.53
4223984-22398482.69283.99
5232629-23262985.88487.20
6226229-22622983.52184.81
极限1250942-25094292.64592.190.9994.2593.750.98
2251004-25100492.66894.22
3245776-24577690.73892.29
4249287-24928792.03493.58
5252802-25280293.33294.90
6248454-24845491.72693.27
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