辅酶Q10片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号140611-202107对照品来源中检所对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数500
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.052728302725172722882720552717922722960.15
210.072710572714132712350.10
单位质量响应值RSD%判断
27094.1326934.960.42数据可信
供试品溶液-24110601批-pH1.2盐酸溶液-乙醇溶液（5：95）
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1178638-17863865.99564.583.5165.9964.583.51
2164119-16411960.63160.63
3175452-17545264.81864.82
4172609-17260963.76863.77
5176013-17601365.02565.03
6182042-18204267.25267.25
10min1193601-19360171.52368.263.0071.7268.453.00
2176911-17691165.35765.54
3186466-18646668.88769.08
4183911-18391167.94368.13
5185888-18588868.67368.87
6181841-18184167.17867.38
15min1195763-19576372.32170.032.3272.7370.432.32
2182545-18254567.43867.82
3190984-19098470.55670.96
4189203-18920369.89870.29
5191211-19121170.64071.04
6187617-18761769.31269.72
20min1198071-19807173.17470.812.6073.8071.422.59
2184259-18425968.07268.65
3193700-19370071.55972.17
4191092-19109270.59671.20
5194875-19487571.99372.61
6188088-18808869.48670.10
30min1201895-20189574.58771.972.2475.4472.802.24
2188788-18878869.74570.53
3195231-19523172.12572.95
4194375-19437571.80972.63
5196274-19627472.51073.34
6192368-19236871.06771.89
45min1202455-20245574.79472.791.9475.8773.831.94
2191650-19165070.80271.80
3199100-19910073.55474.60
4196068-19606872.43473.47
5198450-19845073.31474.36
6194424-19442471.82772.86
60min1205541-20554175.93473.602.1677.2374.862.16
2192511-19251171.12072.33
3200670-20067074.13475.40
4198478-19847873.32474.57
5200556-20055674.09275.36
6197655-19765573.02074.27
极限1250724-25072492.62691.091.4594.1592.561.46
2240692-24069288.92090.34
3246492-24649291.06292.55
4247545-24754591.45292.92
5249259-24925992.08593.57
6244659-24465990.38591.85
辅酶Q10片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号140611-202107对照品来源中检所对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数500
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.052717632716692714652718802709882715530.13
210.072728532730702729620.06
单位质量响应值RSD%判断
27020.2027106.450.23数据可信
供试品溶液-24110602批
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1110729-11072940.83339.882.8340.8339.882.83
2111013-11101340.93840.94
3102711-10271137.87637.88
4106902-10690239.42239.42
5108968-10896840.18440.18
6108555-10855540.03140.03
10min1116720-11672043.04244.293.7843.1644.403.78
2123803-12380345.65445.78
3113538-11353841.86941.98
4118518-11851843.70543.82
5123031-12303145.37045.49
6124964-12496446.08246.20
15min1120482-12048244.43046.474.3444.6846.724.34
2129541-12954147.77048.03
3119098-11909843.91944.16
4124624-12462445.95746.21
5129703-12970347.83048.09
6132577-13257748.89049.15
20min1122484-12248445.16847.614.7245.5548.004.71
2132477-13247748.85349.26
3122185-12218545.05845.43
4127100-12710046.87047.26
5133724-13372449.31349.71
6136628-13662850.38450.79
30min1126153-12615346.52149.504.9847.0450.044.97
2137650-13765050.76151.31
3127224-12722446.91647.42
4132608-13260848.90149.43
5139137-13913751.30951.86
6142608-14260852.58953.15
45min1129870-12987047.89251.215.5848.5551.895.56
2141545-14154552.19752.90
3131089-13108948.34148.99
4136422-13642250.30850.98
5145099-14509953.50854.21
6149193-14919355.01755.73
60min1132033-13203348.68952.285.5549.4953.125.52
2144866-14486653.42254.28
3134458-13445849.58350.38
4139464-13946451.43052.26
5147312-14731254.32455.19
6152487-15248756.23257.11
极限1197845-19784572.95874.622.3973.9175.612.42
2203043-20304374.87575.89
3196006-19600672.28073.22
4203042-20304274.87575.85
5204744-20474475.50376.53
6209387-20938777.21578.26
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