布洛芬混悬液项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)0
对照品批号100179-202308对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数50
标示量(mg)200供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
1 10.772596293258842525870522594728259325725919510.16
2 10.802585709259532025905140.27
单位质量响应值RSD%判断
240663.97239862.410.24数据可信
加速6月-供试品溶液-2025110151批-pH7.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min12603736-260373697.43695.102.7597.4495.102.75
22599472-259947297.27697.28
32575167-257516796.36796.37
42560962-256096295.83595.84
52443313-244331391.43391.43
62464936-246493692.24292.24
10min12590726-259072696.94995.632.1897.4996.162.18
22614788-261478897.84998.39
32587039-258703996.81197.35
42566282-256628296.03496.57
52476940-247694092.69193.20
62497222-249722293.45093.96
15min12575218-257521896.36994.991.8897.4596.061.88
22582356-258235696.63697.72
32564718-256471895.97697.05
42550699-255069995.45196.52
52472029-247202992.50793.53
62485938-248593893.02894.06
20min12576711-257671196.42594.442.0598.0496.032.05
22580274-258027496.55898.18
32545696-254569695.26496.87
42506098-250609893.78295.38
52460754-246075492.08593.62
62473312-247331292.55594.10
30min12558480-255848095.74294.052.0597.8996.162.05
22556561-255656195.67197.83
32539731-253973195.04197.18
42526992-252699294.56496.68
52444853-244485391.49093.54
62452563-245256391.77993.84
极限12533767-253376794.81893.421.7197.5096.051.72
22538663-253866395.00197.69
32507817-250781793.84696.51
42509032-250903293.89296.53
52433804-243380491.07793.63
62455549-245554991.89094.46
布洛芬混悬液项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)0
对照品批号100179-202308对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数50
标示量(mg)200供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
1 10.772590516258828625903232588725259208425899870.06
2 10.802590037258949325897650.02
单位质量响应值RSD%判断
240481.62239793.060.21数据可信
中间条件6月-供试品溶液-2025110251批-pH7.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min12615860-261586097.94196.381.1997.9496.381.19
22594064-259406497.12597.12
32579674-257967496.58696.59
42572599-257259996.32196.32
52554175-255417595.63195.63
62528730-252873094.67994.68
10min12611991-261199197.79696.661.1398.3497.201.13
22610755-261075597.75098.29
32595308-259530897.17197.71
42571707-257170796.28896.82
52560165-256016595.85696.39
62540658-254065895.12595.65
15min12584957-258495796.78496.230.7997.8797.300.79
22591704-259170497.03698.12
32584269-258426996.75897.83
42567562-256756296.13297.20
52550925-255092595.51096.57
62542376-254237695.18996.24
20min12578056-257805696.52595.690.9498.1597.300.94
22578548-257854896.54498.17
32573433-257343396.35297.97
42545612-254561295.31196.91
52529515-252951594.70896.30
62528968-252896894.68796.27
30min12573062-257306296.33895.330.9498.5097.470.94
22570052-257005296.22698.38
32550867-255086795.50797.66
42540121-254012195.10597.24
52532720-253272094.82896.95
62509942-250994293.97596.08
极限12548630-254863095.42494.530.9398.1297.200.93
22546586-254658695.34798.04
32534877-253487794.90997.59
42521397-252139794.40497.07
52508786-250878693.93296.58
62488734-248873493.18195.81
布洛芬混悬液项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)0
对照品批号100179-202308对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数50
标示量(mg)200供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
1 10.772594282258856125938792593084259368125926970.10
2 10.802590766258771725892420.09
单位质量响应值RSD%判断
240733.24239744.630.30数据可信
-供试品溶液-250226083批-pH7.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min12682205-2682205100.38397.752.07100.3897.752.07
22637879-263787998.72498.72
32647872-264787299.09899.10
42601390-260139097.35897.36
52555726-255572695.64995.65
62545555-254555595.26895.27
10min12676056-2676056100.15298.151.92100.7198.701.92
22652339-265233999.26599.81
32659077-265907799.517100.07
42624618-262461898.22798.77
52569158-256915896.15296.68
62554590-255459095.60796.14
15min12665024-266502499.74097.621.90100.8598.711.90
22636126-263612698.65899.76
32641557-264155798.86199.96
42608762-260876297.63498.72
52558870-255887095.76796.83
62540229-254022995.06996.13
20min12648580-264858099.12497.081.90100.7998.711.91
22617254-261725497.95299.60
32632519-263251998.523100.18
42595668-259566897.14498.77
52540044-254004495.06296.66
62529085-252908594.65296.24
30min12635226-263522698.62496.611.83100.8498.781.83
22604123-260412397.46099.65
32616952-261695297.940100.14
42581390-258139096.61098.78
52528676-252867694.63796.76
62521301-252130194.36196.48
极限12623174-262317498.17396.041.91100.9498.751.91
22588298-258829896.86899.60
32602172-260217297.387100.13
42567624-256762496.09498.80
52515784-251578494.15496.81
62499923-249992393.56196.20
布洛芬混悬液项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)0
对照品批号100179-202308对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数50
标示量(mg)200供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
1 10.772588796259063525904692592929259005525905770.06
2 10.802579870258431225820910.13
单位质量响应值RSD%判断
240536.40239082.500.43数据可信
-供试品溶液-250226083批-pH7.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min12640124-264012498.98597.801.6198.9997.801.61
22654079-265407999.50899.51
32630863-263086398.63898.64
42610328-261032897.86897.87
52557082-255708295.87295.87
62557918-255791895.90395.90
10min12688028-2688028100.78198.541.77101.3399.091.76
22666003-266600399.955100.51
32638388-263838898.92099.47
42627107-262710798.49799.04
52580065-258006596.73397.27
62570733-257073396.38396.92
15min12665215-266521599.92698.011.66101.0499.111.66
22650400-265040099.370100.48
32627712-262771298.52099.62
42616123-261612398.08599.18
52565538-256553896.18997.26
62560483-256048395.99997.07
20min12654216-265421699.51397.531.78101.1899.161.78
22647872-264787299.276100.94
32612347-261234797.94499.59
42594659-259465997.28198.92
52553260-255326095.72897.33
62544893-254489395.41597.02
30min12647278-264727899.25397.101.75101.4799.271.75
22628871-262887198.563100.77
32596532-259653297.35199.54
42589737-258973797.09699.27
52543075-254307595.34797.48
62533112-253311294.97397.10
极限12619310-261931098.20596.371.62100.9799.091.62
22607513-260751397.762100.52
32583782-258378296.87399.60
42567008-256700896.24498.96
52523443-252344394.61097.28
62521228-252122894.52797.19
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