叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数2000
标示量(mg)5供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.11 1208198120727812075031207221120711512074630.04
210.141203736120228212030090.09
单位质量响应值RSD%判断
119432.54118639.940.48数据可信
供试品溶液-第3批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min140731-407315.6173.6329.585.623.6329.60
227038-270383.7293.73
319215-192152.6502.65
426818-268183.6983.70
523614-236143.2573.26
620310-203102.8012.80
10min1105121-10512114.4979.0532.7214.569.0832.72
268272-682729.4159.46
357961-579617.9938.02
467306-673069.2829.32
549997-499976.8956.93
644910-449106.1936.22
15min1185685-18568525.60816.7831.8525.8316.9231.84
2141782-14178219.55319.70
3114233-11423315.75415.87
4121477-12147716.75316.90
588124-8812412.15312.27
678918-7891810.88410.98
20min1235134-23513432.42724.5424.4532.9424.8724.51
2206764-20676428.51528.88
3185291-18529125.55325.85
4186780-18678025.75926.09
5130096-13009617.94118.19
6123755-12375517.06717.29
30min1315195-31519543.46837.8114.1544.3438.4114.33
2307642-30764242.42743.11
3286410-28641039.49940.08
4280753-28075338.71839.33
5218313-21831330.10730.55
6236770-23677032.65333.06
45min1392173-39217354.08450.906.9855.4451.927.24
2401819-40181955.41556.57
3371150-37115051.18552.20
4369189-36918950.91551.96
5336538-33653846.41247.19
6343596-34359647.38548.16
60min1440825-44082560.79459.434.0262.7561.024.24
2456745-45674562.98964.76
3433372-43337259.76661.35
4423064-42306458.34459.96
5426006-42600658.75060.05
6405673-40567355.94657.25
90min1488456-48845667.36367.853.2969.9970.093.36
2524077-52407772.27574.74
3485100-48510066.90069.15
4479454-47945466.12168.38
5490312-49031267.61869.57
6484345-48434566.79668.72
极限1538491-53849174.26374.772.9577.6477.773.05
2571501-57150178.81582.09
3548317-54831775.61878.61
4528297-52829772.85775.85
5531236-53123673.26275.96
6535199-53519973.80976.47
叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数2000
标示量(mg)5供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.11 1204565120324312032481202854120311012034040.06
210.141200882119989312003880.06
单位质量响应值RSD%判断
119031.06118381.460.39数据可信
供试品溶液-第4批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min147472-474726.5655.0723.646.565.0823.59
245553-455536.3006.30
332290-322904.4654.47
435833-358334.9554.96
524130-241303.3373.34
634866-348664.8224.82
10min1125363-12536317.33713.4921.2217.4113.5421.23
2119657-11965716.54816.62
374085-7408510.24510.29
495767-9576713.24413.30
582285-8228511.37911.42
687998-8799812.16912.22
15min1195345-19534527.01522.6317.2727.2822.8317.29
2196931-19693127.23427.49
3126272-12627217.46217.63
4163140-16314022.56122.76
5157294-15729421.75221.92
6142709-14270919.73619.92
20min1252871-25287134.97030.5014.2935.5430.9614.33
2253261-25326135.02435.58
3173381-17338123.97724.33
4221171-22117130.58631.04
5226322-22632231.29931.70
6196304-19630427.14727.56
30min1327190-32719045.24843.009.7246.2043.809.78
2329371-32937145.54946.49
3259166-25916635.84136.46
4337082-33708246.61647.41
5323109-32310944.68345.44
6289812-28981240.07940.79
45min1406073-40607356.15754.644.1957.6155.924.31
2399924-39992455.30656.76
3368678-36867850.98552.01
4391404-39140454.12855.44
5416620-41662057.61558.86
6387961-38796153.65254.81
60min1452947-45294762.63962.562.2164.7264.442.27
2450266-45026662.26864.33
3440353-44035360.89762.49
4447876-44787661.93863.85
5470507-47050765.06766.96
6452274-45227462.54664.30
90min1497611-49761168.81671.052.9571.5973.622.76
2505208-50520869.86672.62
3513440-51344071.00573.27
4504383-50438369.75272.35
5539069-53906974.54977.16
6522771-52277172.29574.74
极限1541798-54179874.92676.352.4978.4779.712.33
2536754-53675474.22977.76
3552644-55264476.42679.48
4547902-54790275.77079.15
5575448-57544879.58083.02
6557803-55780377.14080.39
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