贝派度酸片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号BEMA-231010D对照品来源自制对照品使用方法直接使用
对照品含量(%)99.72对照品水分(%)0对照品稀释倍数50
标示量(mg)180供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.26 3051303051163049723049843049393050280.03
210.253048313050733049520.06
单位质量响应值RSD%判断
29729.8229751.410.06数据可信
供试品溶液-2024090421批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1145866-14586648.90950.599.3748.9150.599.37
2177651-17765159.56659.57
3147735-14773549.53549.54
4138217-13821746.34446.34
5153698-15369851.53551.53
6142072-14207247.63747.64
10min1262821-26282188.12488.921.0288.2189.011.03
2266015-26601589.19589.29
3269654-26965490.41590.50
4265093-26509388.88588.96
5265655-26565589.07489.16
6262018-26201887.85487.93
15min1282850-28285094.83995.430.7595.0795.660.75
2284174-28417495.28395.53
3288147-28814796.61596.85
4286123-28612395.93796.16
5283660-28366095.11195.35
6282735-28273594.80195.03
20min1288292-28829296.66497.600.7497.0597.990.74
2289532-28953297.08097.49
3293928-29392898.55498.95
4292352-29235298.02598.41
5289966-28996697.22597.62
6292428-29242898.05198.43
30min1291657-29165797.79298.790.7698.3499.340.75
2293432-29343298.38798.96
3297872-29787299.876100.43
4296453-29645399.40099.95
5293976-29397698.57099.12
6294345-29434598.69499.24
45min1293108-29310898.27999.400.6898.99100.120.68
2295926-29592699.22499.96
3298763-298763100.175100.90
4298248-298248100.002100.72
5296621-29662199.457100.18
6296015-29601599.25499.97
60min1293795-29379598.50999.650.7999.38100.540.79
2296725-29672599.492100.39
3299696-299696100.488101.38
4298829-298829100.197101.08
5298873-298873100.212101.10
6295326-29532699.02399.90
极限1295843-29584399.19699.900.55100.23100.950.55
2299804-299804100.524101.59
3299118-299118100.294101.35
4298181-29818199.980101.03
5298613-298613100.125101.18
6296157-29615799.301100.34
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