苯磺酸氨氯地平缬沙坦片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100374-202106对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数2000
标示量(mg)5供试品稀释倍数1系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.172466462467272465072463562459522464380.13
214.092412702411922412310.03
单位质量响应值RSD%判断
17391.5317120.721.11数据可信
加速6月-供试品溶液-2023112221批-苯磺酸氨氯地平-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min191903-9190334.52733.234.0834.5333.234.08
288509-8850933.25233.25
388519-8851933.25533.26
483732-8373231.45731.46
585120-8512031.97931.98
692887-9288734.89634.90
10min1134121-13412150.38849.801.2450.4549.861.24
2134579-13457950.56050.62
3131652-13165249.46049.52
4133101-13310150.00450.06
5130490-13049049.02349.08
6131368-13136849.35349.41
15min1165959-16595962.34961.371.1962.4961.501.19
2162874-16287461.19061.33
3164710-16471061.87962.02
4164112-16411261.65561.79
5161438-16143860.65060.79
6160955-16095560.46960.61
20min1185487-18548769.68568.381.4169.9368.621.41
2181193-18119368.07268.31
3180339-18033967.75167.99
4185067-18506769.52769.77
5180211-18021167.70367.94
6179825-17982567.55867.80
30min1207011-20701177.77176.880.7878.1377.240.78
2203368-20336876.40376.76
3203282-20328276.37076.72
4203412-20341276.41976.77
5206067-20606777.41777.77
6204722-20472276.91177.27
45min1227226-22722685.36683.701.6985.8684.181.69
2219090-21909082.30982.79
3221758-22175883.31283.79
4227634-22763485.51986.00
5221630-22163083.26483.74
6219378-21937882.41882.90
60min1232121-23212187.20586.601.3587.8487.221.34
2226552-22655285.11385.73
3230189-23018986.47987.10
4235470-23547088.46389.09
5228278-22827885.76186.38
6230395-23039586.55787.18
极限1245784-24578492.33892.351.2993.1293.121.29
2243200-24320091.36792.13
3249743-24974393.82594.59
4247857-24785793.11793.89
5241120-24112090.58691.35
6247125-24712592.84293.61
苯磺酸氨氯地平缬沙坦片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100651-202307对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.1对照品水分(%)0对照品稀释倍数200
标示量(mg)80供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
116.044729490473261647347834732471472782747314370.06
216.064648594464809646483450.01
单位质量响应值RSD%判断
294977.37289436.181.35数据可信
加速6月-供试品溶液-2023112221批-缬沙坦-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min13722243-372224371.01569.171.8371.0169.171.82
23667251-366725169.96669.97
33641922-364192269.48369.48
43578543-357854368.27368.27
53606555-360655568.80868.81
63536849-353684967.47867.48
10min14375223-437522383.47382.852.9783.5982.962.97
24388156-438815683.72083.84
34409978-440997884.13684.25
44441180-444118084.73184.84
54354303-435430383.07483.19
64086428-408642877.96378.08
15min14604330-460433087.84487.982.3388.1088.242.33
24618464-461846488.11488.37
34691596-469159689.50989.76
44716301-471630189.98090.24
54627794-462779488.29288.54
64411671-441167184.16884.41
20min14737382-473738290.38290.762.1990.7991.162.19
24754111-475411190.70191.10
34841820-484182092.37592.78
44876014-487601493.02793.43
54756108-475610890.74091.14
64577520-457752087.33287.72
30min14828586-482858692.12293.352.3492.6893.902.33
24875487-487548793.01793.57
34991238-499123895.22595.78
45052518-505251896.39596.95
54876848-487684893.04393.59
64734303-473430390.32490.85
45min15054840-505484096.43995.122.3497.1595.822.33
24926785-492678593.99694.71
35072872-507287296.78397.50
45120922-512092297.70098.42
54923825-492382593.93994.65
64813583-481358391.83692.51
60min14874603-487460393.00094.912.2193.8795.772.20
24925093-492509393.96494.83
35093179-509317997.17098.05
45132409-513240997.91998.80
54925986-492598693.98194.84
64896282-489628293.41494.25
极限15041672-504167296.18897.141.7797.2198.171.76
25049628-504962896.33997.36
35225554-522555499.696100.74
45174220-517422098.71799.76
54987336-498733695.15196.17
65072293-507229396.77297.76
点击查看处理图标(人工保存)
　
原始图谱下载图谱(王丹 于 2024-09-26 15:05:21 完成)
生成报告数据部分(等待生成报告)
Current page cost:38 ms