非奈利酮片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号FN-706-231101对照品来源自制对照品使用方法直接使用
对照品含量(%)100.0对照品水分(%)0对照品稀释倍数1000
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.091853131853621851261851391850831852050.07
211.071852361850871851620.06
单位质量响应值RSD%判断
16700.1816726.470.12数据可信
供试品溶液-24092401批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min191003-9100349.00438.7922.9549.0038.7922.95
264144-6414434.54134.54
356342-5634230.34030.34
452603-5260328.32628.33
587999-8799947.38747.39
680092-8009243.12943.13
10min1138538-13853874.60271.155.5574.6871.225.57
2126248-12624867.98468.04
3127256-12725668.52668.58
4123345-12334566.42066.47
5140373-14037375.59075.67
6137048-13704873.79973.87
15min1151972-15197281.83681.743.1982.0481.923.20
2149267-14926780.37980.55
3150381-15038180.97981.14
4144822-14482277.98678.14
5156116-15611684.06784.27
6158186-15818685.18285.38
20min1158157-15815785.16686.792.6385.5187.112.64
2160324-16032486.33386.64
3162821-16282187.67887.98
4154931-15493183.42983.72
5164311-16431188.48088.83
6166499-16649989.65990.00
30min1165781-16578189.27291.862.2489.7692.332.24
2172138-17213892.69593.14
3172810-17281093.05793.50
4165930-16593089.35289.78
5171988-17198892.61493.11
6174919-17491994.19394.68
45min1170540-17054091.83595.432.4492.4796.052.42
2179585-17958596.70597.31
3179726-17972696.78197.38
4173719-17371993.54694.12
5177649-17764995.66396.31
6182101-18210198.06098.70
60min1172298-17229892.78196.842.4793.5797.622.45
2183485-18348598.80599.57
3182931-18293198.50799.27
4176859-17685995.23795.97
5180622-18062297.26498.07
6182840-18284098.45899.26
极限1175495-17549594.50398.682.3595.4499.622.33
2187464-187464100.948101.88
3186280-186280100.310101.24
4181870-18187097.93698.83
5183293-18329398.70299.67
6185100-18510099.675100.65
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