叶酸左氨氯地平片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100546-202105 对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数5000
标示量(mg)2.5供试品稀释倍数1系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
117.537607876056762807633876269762040.17
217.497470774563746350.14
单位质量响应值RSD%判断
4347.064267.301.31数据可信
供试品溶液-24091401批-左氨氯地平-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min148415-4841556.78155.433.4956.7855.423.50
246496-4649654.53154.53
347024-4702455.15055.15
444742-4474252.47452.47
547319-4731955.49655.50
649559-4955958.12358.12
10min162140-6214072.87875.462.5773.5176.082.56
263351-6335174.29874.90
366002-6600277.40778.02
463183-6318374.10174.68
565852-6585277.23177.85
665520-6552076.84277.49
15min168945-6894580.85981.261.7282.3082.711.72
268229-6822980.01981.45
369806-6980681.86983.34
467992-6799279.74181.15
571255-7125583.56885.04
669481-6948181.48782.99
20min170798-7079883.03283.753.2885.3786.113.24
269240-6924081.20583.53
372608-7260885.15587.54
468673-6867380.54082.83
574989-7498987.94790.35
672170-7217084.64187.05
30min173413-7341386.09987.103.6389.3690.383.57
270107-7010782.22285.44
376505-7650589.72593.05
473156-7315685.79888.98
577688-7768891.11394.49
674726-7472687.63990.98
45min174901-7490187.84489.722.3992.0693.972.34
274248-7424887.07891.21
378453-7845392.01096.34
478088-7808891.58295.72
577813-7781391.25995.65
675495-7549588.54192.86
极限177922-7792291.38795.232.4296.58100.482.38
281027-8102795.029100.13
382209-8220996.415101.76
480249-8024994.11699.27
583544-8354497.981103.39
682243-8224396.455101.76
叶酸左氨氯地平片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217 对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数20000
标示量(mg)0.8供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.769361093069930959299092724930980.35
214.829222392034921280.15
单位质量响应值RSD%判断
6307.456216.461.03数据可信
供试品溶液-24091401批-叶酸-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1113884-11388493.30291.433.5793.3091.433.57
2110546-11054690.56890.57
3105081-10508186.09086.09
4117003-11700395.85895.86
5110853-11085390.81990.82
6112197-11219791.92091.92
10min1117347-11734796.14094.323.7097.1895.343.69
2114969-11496994.19195.20
3108144-10814488.60089.56
4120090-12009098.38799.45
5112669-11266992.30793.32
6117557-11755796.31297.33
15min1119684-11968498.05494.853.64100.1696.913.64
2114888-11488894.12596.18
3109537-10953789.74191.68
4121247-12124799.335101.49
5113920-11392093.33295.37
6115337-11533794.49396.58
20min1117826-11782696.53294.263.7099.7397.373.69
2115056-11505694.26397.36
3107804-10780488.32191.26
4120451-12045198.683101.94
5114051-11405193.43996.51
6115096-11509694.29597.44
30min1116630-11663095.55294.233.2699.8298.393.27
2115269-11526994.43798.58
3109196-10919689.46293.38
4120564-12056498.775103.13
5113346-11334692.86296.97
6115065-11506594.27098.46
45min1117283-11728396.08793.833.29101.4299.043.30
2114453-11445393.76998.96
3108631-10863188.99993.91
4119658-11965898.033103.49
5113270-11327092.79997.94
6113883-11388393.30298.54
极限1118722-11872297.26693.723.63103.6699.973.61
2112956-11295692.54298.78
3107895-10789588.39694.30
4119041-11904197.527104.07
5113294-11329492.81998.99
6114437-11443793.755100.03
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