叶酸左氨氯地平片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100546-202105 对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数5000
标示量(mg)2.5供试品稀释倍数1系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
117.537813877428778057745177508776660.40
217.497794877535777420.38
单位质量响应值RSD%判断
4430.464444.940.24数据可信
供试品溶液-24091401批-左氨氯地平-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min150098-5009857.02254.713.7557.0254.713.75
247283-4728353.81853.82
347321-4732153.86153.86
450257-5025757.20357.20
547834-4783454.44554.45
645603-4560351.90651.91
10min163474-6347472.24774.181.6172.8874.791.59
266001-6600175.12375.72
364691-6469173.63274.23
465126-6512674.12774.76
566468-6646875.65576.26
665298-6529874.32374.90
15min169164-6916478.72379.142.0580.1680.572.03
269516-6951679.12480.56
368514-6851477.98479.40
469567-6956779.18280.64
572202-7220282.18183.63
668197-6819777.62379.03
20min171203-7120381.04481.672.7683.3683.982.72
273317-7331783.45085.76
369902-6990279.56381.85
472084-7208482.04784.39
574576-7457684.88387.24
669439-6943979.03681.30
30min174343-7434384.61884.983.9287.8388.203.83
276191-7619186.72289.96
369787-6978779.43382.60
475435-7543585.86189.11
578521-7852189.37492.68
673685-7368583.86987.01
45min174668-7466884.98887.282.2589.1491.442.19
278534-7853489.38893.59
374526-7452684.82688.88
476735-7673587.34191.55
577489-7748988.19992.49
678123-7812388.92193.00
极限178217-7821789.02893.002.5194.1298.132.44
282198-8219893.55998.75
381693-8169392.98497.98
483056-8305694.53599.71
584168-8416895.801101.08
680905-8090592.08797.15
叶酸左氨氯地平片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217 对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数20000
标示量(mg)0.8供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.769263892349911679271191923921580.69
214.829170691622916640.07
单位质量响应值RSD%判断
6243.776185.160.67数据可信
供试品溶液-24091401批-叶酸-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1115569-11556995.40493.152.8295.4093.152.82
2107847-10784789.02989.03
3112728-11272893.05893.06
4113044-11304493.31993.32
5111114-11111491.72691.73
6116711-11671196.34696.35
10min1116435-11643596.11995.992.7397.1897.032.72
2111591-11159192.12093.11
3115392-11539295.25896.29
4115446-11544695.30296.34
5117534-11753497.02698.04
6121299-121299100.134101.20
15min1118932-11893298.18096.123.70100.3198.223.67
2110359-11035991.10393.12
3115295-11529595.17797.27
4116914-11691496.51498.61
5114171-11417194.25096.35
6122960-122960101.505103.69
20min1117292-11729296.82696.024.50100.0499.194.45
2107870-10787089.04892.07
3116720-11672096.35499.50
4117831-11783197.271100.44
5114287-11428794.34597.49
6123904-123904102.284105.60
30min1116678-11667896.31995.523.78100.6199.763.75
2108839-10883989.84893.86
3117671-11767197.139101.36
4115914-11591495.68899.94
5113347-11334793.56997.76
6121840-121840100.580105.03
45min1118346-11834697.69695.883.08103.06101.183.09
2109973-10997390.78495.80
3115386-11538695.253100.55
4117696-11769697.159102.47
5115192-11519295.092100.32
6120286-12028699.298104.86
极限1119175-11917598.38094.813.93104.83101.173.87
2108775-10877589.79595.82
3112515-11251592.88399.24
4114559-11455994.570100.96
5113100-11310093.36599.65
6120945-12094599.842106.51
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