左氨氯地平叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100546-202105 对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数5000
标示量(mg)2.5供试品稀释倍数1系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
117.267508574849752207522175173751100.21
217.217475774723747400.04
单位质量响应值RSD%判断
4351.684342.820.15数据可信
供试品溶液-24082901批-左氨氯地平-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min146687-4668754.24555.543.6754.2555.543.67
248222-4822256.02956.03
345758-4575853.16653.17
450772-5077258.99258.99
548341-4834156.16756.17
647005-4700554.61554.61
10min157802-5780267.16070.475.8267.7671.095.80
262065-6206572.11372.74
355564-5556464.55965.15
465621-6562176.24576.90
561058-6105870.94371.57
661809-6180971.81572.42
15min159231-5923168.82073.685.9170.1775.085.88
264730-6473075.20976.63
359775-5977569.45270.76
469510-6951080.76382.27
564013-6401374.37675.79
663211-6321173.44474.85
20min162314-6231472.40275.255.2974.5277.485.28
265555-6555576.16878.43
360720-6072070.55072.63
470520-7052081.93784.34
565851-6585176.51278.75
663650-6365073.95576.18
30min162251-6225172.32975.523.8575.2578.573.89
264349-6434974.76777.87
362912-6291273.09775.96
469206-6920680.41083.72
566118-6611876.82279.91
665129-6512975.67378.72
45min163720-6372074.03676.214.8477.7680.104.82
267286-6728678.17982.12
361326-6132671.25474.93
469501-6950180.75384.96
568112-6811279.13983.08
663577-6357773.87077.75
极限174281-7428186.30787.571.4990.8592.311.59
274469-7446986.52591.33
375413-7541387.62292.09
477120-7712089.60594.71
576226-7622688.56693.39
674713-7471386.80991.51
左氨氯地平叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217 对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数20000
标示量(mg)0.8供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
116.20 9517495466954579533195060952980.19
216.27 9377193727937490.04
单位质量响应值RSD%判断
5882.595762.081.47数据可信
供试品溶液-24082901批-叶酸-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1113812-113812100.28999.851.93100.2999.851.93
2109782-10978296.73896.74
3115887-115887102.118102.12
4115150-115150101.468101.47
5112438-11243899.07999.08
6112828-11282899.42299.42
10min1115146-115146101.465101.311.68102.58102.421.68
2114021-114021100.474101.55
3118187-118187104.145105.28
4115998-115998102.216103.34
5113483-11348399.999101.10
6112980-11298099.556100.66
15min1113917-113917100.382100.451.69102.62102.681.68
2113313-11331399.850102.04
3117262-117262103.329105.62
4114795-114795101.156103.42
5113077-11307799.642101.85
6111599-11159998.339100.55
20min1112960-11296099.53999.141.82102.90102.491.81
2111878-11187898.585101.89
3115892-115892102.122105.56
4113076-11307699.641103.03
5111412-11141298.174101.49
6109817-10981796.769100.07
30min1111552-11155298.29897.811.93102.76102.261.92
2110314-11031497.207101.60
3114667-114667101.043105.62
4111237-11123798.020102.51
5109941-10994196.878101.29
6108277-10827795.41299.79
45min1110350-11035097.23996.952.48102.79102.492.43
2108846-10884695.913101.39
3115182-115182101.497107.19
4109792-10979296.747102.33
5108435-10843595.551101.04
6107525-10752594.749100.19
极限1109932-10993296.87096.872.60103.51103.492.53
2108435-10843595.551102.09
3114888-114888101.237108.06
4108775-10877595.851102.51
5111007-11100797.818104.37
6106573-10657393.910100.40
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