盐酸司来吉兰片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号101298-201801对照品来源中检院对照品使用方法减压干燥3h
对照品含量(%)99.5对照品水分(%)0对照品稀释倍数1000
标示量(mg)5供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.182514242514742514562516612510922514210.09
210.152519372516272517820.09
单位质量响应值RSD%判断
24697.5424806.110.32数据可信
供试品溶液-24102101批-水
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1168502-16850267.73774.3111.9067.7474.3111.90
2175184-17518470.42370.42
3191757-19175777.08577.08
4176883-17688371.10671.11
5226488-22648891.04691.05
6170249-17024968.43968.44
10min1208644-20864483.87389.156.4684.0889.386.47
2216165-21616586.89787.11
3235566-23556694.69694.93
4218422-21842287.80488.02
5242999-24299997.68497.96
6208833-20883383.94984.15
15min1227045-22704591.27093.603.7491.7394.093.76
2227466-22746691.44091.91
3242040-24204097.29897.81
4231362-23136293.00693.48
5245120-24512098.53699.10
6223988-22398890.04190.50
20min1231550-23155093.08194.882.8393.8195.652.86
2229870-22987092.40693.15
3243908-24390898.04998.86
4234304-23430494.18894.94
5244935-24493598.46299.32
6231599-23159993.10193.83
30min1234376-23437694.21795.292.4495.2396.342.46
2228749-22874991.95592.98
3244315-24431598.21399.31
4234981-23498194.46195.50
5242785-24278597.59898.75
6237038-23703895.28796.29
45min1234604-23460494.30995.092.2795.6096.432.29
2227696-22769691.53292.83
3241363-24136397.02698.42
4235339-23533994.60595.93
5242441-24244197.45998.91
6237786-23778695.58896.88
60min1234373-23437394.21694.852.6895.7996.482.69
2224895-22489590.40691.98
3241796-24179697.20098.89
4234496-23449694.26695.87
5241456-24145697.06398.81
6238733-23873395.96997.55
极限1233176-23317693.73594.622.4395.5996.532.44
2226168-22616890.91892.76
3241186-24118696.95598.93
4232801-23280193.58495.47
5239894-23989496.43698.47
6238996-23899696.07597.94
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