苯磺酸左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)10补液体积(ml)10
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数10000
标示量(mg)2.5供试品稀释倍数5系数0.7211
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.608703787878876898789286931874850.54
214.678674187567871540.68
单位质量响应值RSD%判断
5992.125940.970.61数据可信
供试品溶液-2024101922批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min162290-6229073.25169.9212.4573.2569.9212.45
250139-5013958.96258.96
358588-5858868.89768.90
452031-5203161.18661.19
569443-6944381.66281.66
664281-6428175.59275.59
10min172166-7216684.86480.835.5586.3382.235.66
264287-6428775.59976.78
367920-6792079.87181.25
464268-6426875.57776.80
572421-7242185.16486.80
671348-7134883.90385.41
15min172155-7215584.85280.187.0788.0183.197.11
259866-5986670.40073.09
368878-6887880.99883.97
465254-6525476.73679.47
572025-7202584.69988.04
670891-7089183.36586.56
20min170780-7078083.23579.854.5188.0984.464.68
264245-6424575.55079.65
367149-6714978.96583.56
464444-6444475.78480.05
570076-7007682.40787.44
670702-7070283.14388.00
30min169993-6999382.30979.683.8988.8385.904.11
264341-6434175.66381.27
367118-6711878.92885.10
465054-6505476.50182.29
570015-7001582.33589.01
670039-7003982.36388.88
45min169501-6950181.73179.904.0889.9087.714.27
263884-6388475.12582.25
366848-6684878.61186.36
466121-6612177.75685.07
570317-7031782.69091.02
670997-7099783.49091.66
60min167988-6798879.95178.112.9589.7687.523.22
264434-6443475.77284.40
364562-6456275.92285.25
464993-6499376.42985.30
567904-6790479.85389.83
668673-6867380.75790.59
极限175255-7525588.49787.461.8099.9098.431.49
274763-7476387.91898.06
372784-7278485.59196.44
475942-7594289.30599.70
572697-7269785.48997.07
674801-7480187.96399.42
苯磺酸左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)10补液体积(ml)10
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数10000
标示量(mg)2.5供试品稀释倍数5系数0.7211
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.608672186173864958725686232865750.51
214.678736887158872630.18
单位质量响应值RSD%判断
5929.795948.400.23数据可信
供试品溶液-2024101923批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min160344-6034471.28975.216.2771.2975.216.28
265650-6565077.55777.56
364621-6462176.34276.34
467496-6749679.73879.74
566571-6657178.64678.65
657291-5729167.68267.68
10min166741-6674178.84680.343.6480.2781.843.68
268024-6802480.36281.91
367922-6792280.24281.77
470612-7061283.41985.01
570645-7064583.45885.03
664101-6410175.72877.08
15min165597-6559777.49580.573.1480.5083.683.19
268869-6886981.36084.52
368022-6802280.36083.49
470453-7045383.23286.49
570428-7042883.20286.44
665844-6584477.78780.65
20min165390-6539077.25079.593.0581.8084.313.10
267937-6793780.25985.04
366742-6674278.84883.59
470533-7053383.32688.25
568498-6849880.92285.83
665102-6510276.91081.33
30min163453-6345374.96277.673.3881.0683.993.35
266300-6630078.32584.72
365967-6596777.93284.25
469709-6970982.35388.95
564934-6493476.71283.24
664122-6412275.75281.71
45min164603-6460376.32177.031.0383.9284.900.91
266115-6611578.10786.06
365597-6559777.49585.37
464756-6475676.50184.74
564505-6450576.20584.26
665644-6564477.55085.03
60min164613-6461376.33278.161.9785.4687.561.84
266091-6609178.07887.60
365618-6561877.52086.94
467809-6780980.10889.88
565193-6519377.01886.60
667611-6761179.87488.90
极限176216-7621690.04088.582.54100.6999.552.11
272671-7267185.85296.93
375410-7541089.088100.06
475578-7557889.286100.66
572685-7268585.86896.99
677314-7731491.337101.96
苯磺酸左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)10补液体积(ml)10
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数10000
标示量(mg)2.5供试品稀释倍数5系数0.7211
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.608703087240863248730487066869930.45
214.678618787287867370.90
单位质量响应值RSD%判断
5958.425912.540.55数据可信
供试品溶液-2024102021批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min163020-6302074.49774.461.7274.5074.461.72
263220-6322074.73374.73
362054-6205473.35573.35
464355-6435576.07576.07
561462-6146272.65572.65
663821-6382175.44475.44
10min173150-7315086.47281.646.0787.9683.135.97
262444-6244473.81675.31
367339-6733979.60281.07
469390-6939082.02783.55
568187-6818780.60582.06
673885-7388587.34088.85
15min172655-7265585.88682.313.9389.1185.433.91
266767-6676778.92681.90
366998-6699879.19982.26
469048-6904881.62284.78
569133-6913381.72384.79
673166-7316686.49089.75
20min172116-7211685.24980.693.5090.1985.463.46
266370-6637078.45783.01
365728-6572877.69882.34
469484-6948482.13886.93
566971-6697179.16783.87
668876-6887681.41986.40
30min170570-7057083.42279.242.9290.0685.622.81
267608-6760879.92086.04
365373-6537377.27883.48
467175-6717579.40885.85
565854-6585477.84784.13
665596-6559677.54284.16
45min171172-7117284.13379.914.4092.4487.874.22
267817-6781780.16787.88
364367-6436776.08983.83
465349-6534977.25085.28
565749-6574977.72385.56
671133-7113384.08792.25
60min169160-6916081.75580.132.3991.7589.702.42
267970-6797080.34889.67
365704-6570477.67086.93
467364-6736479.63289.20
566519-6651978.63388.03
670019-7001982.77092.62
极限176494-7649490.42489.691.67102.05100.861.64
277631-7763191.769102.70
373993-7399387.46898.29
475190-7519088.883100.05
575493-7549389.241100.21
676460-7646090.384101.89
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