贝派度酸片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号BEMA-231010D对照品来源自制对照品使用方法直接使用
对照品含量(%)99.72对照品水分(%)0对照品稀释倍数50
标示量(mg)180供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.86 3001703003793000443009173012083005440.17
29.933015543018293016920.07
单位质量响应值RSD%判断
30481.1430381.870.24数据可信
供试品溶液-2024090421批-pH6.6
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1224070-22407073.42570.229.2073.4270.229.20
2204702-20470267.07867.08
3211178-21117869.20069.20
4215734-21573470.69370.69
5185482-18548260.78060.78
6244493-24449380.11780.12
10min1261882-26188285.81586.541.5685.9486.661.56
2266915-26691587.46587.58
3257157-25715784.26784.38
4263804-26380486.44586.56
5266546-26654687.34487.45
6268266-26826687.90788.04
15min1275819-27581990.38290.031.0090.6590.291.00
2273129-27312989.50189.76
3273771-27377189.71189.97
4270996-27099688.80289.06
5275750-27575090.36090.61
6278915-27891591.39791.68
20min1285958-28595893.70591.971.2394.1292.381.23
2277553-27755390.95191.36
3279813-27981391.69192.10
4279392-27939291.55391.96
5277528-27752890.94291.34
6283652-28365292.94993.38
30min1292005-29200595.68693.351.2996.2693.921.29
2283297-28329792.83393.39
3283798-28379892.99793.56
4283968-28396893.05393.62
5281507-28150792.24692.80
6284628-28462893.26993.86
45min1293090-29309096.04293.791.2596.7794.511.25
2285730-28573093.63094.34
3284905-28490593.36094.07
4284882-28488293.35294.07
5282702-28270292.63893.34
6286032-28603293.72994.47
60min1284166-28416693.11893.331.3994.0194.201.39
2279802-27980291.68892.56
3283812-28381293.00293.87
4285009-28500993.39494.27
5284091-28409193.09393.95
6291921-29192195.65996.56
极限1292559-29255995.86893.031.5396.9194.061.52
2282760-28276092.65793.68
3282577-28257792.59793.62
4282255-28225592.49193.52
5280579-28057991.94292.95
6282732-28273292.64893.71
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