贝派度酸片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号BEMA-231010D对照品来源自制对照品使用方法直接使用
对照品含量(%)99.72对照品水分(%)0对照品稀释倍数50
标示量(mg)180供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
1 9.862980792978292979812979842979432979630.04
2 9.932987722986092986900.04
单位质量响应值RSD%判断
30219.3730079.560.33数据可信
供试品溶液-2024090421批-pH6.6
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1117750-11775038.94641.034.7738.9541.044.77
2119690-11969039.58839.59
3125833-12583341.62041.62
4131597-13159743.52643.53
5129992-12999242.99543.00
6119525-11952539.53339.53
10min1235847-23584778.00777.222.4878.0777.292.47
2232505-23250576.90276.97
3239494-23949479.21479.28
4227433-22743375.22475.30
5226197-22619774.81674.89
6239323-23932379.15779.22
15min1268096-26809688.67487.951.6588.8788.151.64
2265928-26592887.95788.15
3270467-27046789.45889.66
4260467-26046786.15086.35
5260809-26080986.26486.46
6269659-26965989.19189.39
20min1278544-27854492.13092.371.4092.4792.721.40
2279368-27936892.40292.74
3285230-28523094.34194.69
4275148-27514891.00691.35
5275382-27538291.08491.42
6282017-28201793.27893.62
30min1291253-29125396.33396.130.8696.8396.630.86
2290331-29033196.02896.52
3293331-29333197.02097.53
4289521-28952195.76096.25
5286556-28655694.78095.27
6292859-29285996.86497.37
45min1295539-29553997.75197.521.0298.4198.181.03
2295649-29564997.78798.44
3297762-29776298.48699.16
4291459-29145996.40197.05
5290886-29088696.21296.86
6297738-29773898.47899.14
60min1296997-29699798.23397.901.0999.0598.721.09
2296906-29690698.20399.02
3298455-29845598.71599.55
4292362-29236296.70097.51
5291703-29170396.48297.29
6299506-29950699.06399.89
极限1298932-29893298.87398.660.4899.8699.640.48
2299685-29968599.122100.10
3299309-29930998.998100.00
4296057-29605797.92298.90
5297032-29703298.24599.22
6298657-29865798.78299.77
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