叶酸片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数2000
标示量(mg)5供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.091237859123645312370401236251123979912374800.12
210.041234058123384812339530.02
单位质量响应值RSD%判断
122644.20122903.690.15数据可信
供试品溶液-24102401批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min179762-797625.3325.5110.075.335.5110.03
291874-918746.1426.14
386650-866505.7935.79
485060-850605.6875.69
567552-675524.5164.52
683655-836555.5935.59
10min1147472-1474729.8599.865.419.879.875.38
2144330-1443309.6499.66
3155782-15578210.41510.42
4156931-15693110.49210.50
5135638-1356389.0689.08
6144494-1444949.6609.67
15min1196159-19615913.11413.174.8913.1413.194.89
2206709-20670913.81913.85
3201847-20184713.49413.52
4205482-20548213.73713.76
5182577-18257712.20612.23
6188938-18893812.63112.66
20min1230756-23075615.42715.603.4415.4715.653.45
2244867-24486716.37016.42
3232207-23220715.52415.57
4240170-24017016.05616.11
5222425-22242514.87014.91
6229604-22960415.35015.40
30min1292909-29290919.58219.332.3919.6619.412.40
2298299-29829919.94320.02
3291176-29117619.46619.54
4290869-29086919.44619.52
5280453-28045318.75018.82
6281527-28152718.82118.89
45min1345942-34594223.12823.102.8123.2323.212.80
2351107-35110723.47323.58
3341793-34179322.85022.96
4356106-35610623.80723.92
5349862-34986223.39023.49
6328355-32835521.95222.06
60min1386550-38655025.84325.194.6425.9925.344.62
2393828-39382826.32926.48
3388533-38853325.97526.12
4364777-36477724.38724.54
5379572-37957225.37625.51
6347632-34763223.24123.38
90min1419892-41989228.07228.561.5228.2628.751.51
2436021-43602129.15029.34
3427649-42764928.59028.78
4427101-42710128.55428.74
5432632-43263228.92329.10
6420166-42016628.09028.27
极限1475227-47522731.77131.611.5632.0131.851.58
2482144-48214432.23432.48
3475428-47542831.78532.02
4474590-47459031.72931.97
5469311-46931131.37631.60
6460338-46033830.77631.00
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