替米沙坦左氨氯地平片项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号100629-202204对照品来源中检院对照品使用方法直接使用
对照品含量(%)100.0对照品水分(%)0对照品稀释倍数1250
标示量(mg)80供试品稀释倍数10系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.137457917462837463147459907453687459490.06
211.167438347436967437650.02
单位质量响应值RSD%判断
67021.4766645.610.40数据可信
供试品溶液-2024070521批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1218986-21898629.49029.496.2529.4929.496.25
2239585-23958532.26332.26
3216862-21686229.20429.20
4202456-20245627.26427.26
5228715-22871530.80030.80
6207239-20723927.90827.91
10min1404529-40452954.47554.676.3554.6454.846.35
2419837-41983756.53756.72
3444930-44493059.91660.08
4373684-37368450.32250.47
5410472-41047255.27655.45
6382579-38257951.52051.67
15min1555776-55577674.84376.144.0575.3176.604.05
2551111-55111174.21574.71
3604584-60458481.41681.91
4539168-53916872.60773.04
5575257-57525777.46677.94
6566409-56640976.27576.72
20min1648161-64816187.28489.325.0088.1790.224.98
2643110-64311086.60487.51
3725333-72533397.67698.62
4654547-65454788.14488.98
5674004-67400490.76491.67
6634702-63470285.47286.34
30min1730309-73030998.34698.911.7699.71100.301.74
2758882-758882102.194103.58
3727236-72723697.93299.42
4733101-73310198.722100.05
5735565-73556599.054100.47
6721803-72180397.20198.54
45min1710944-71094495.73998.662.6797.65100.592.67
2726218-72621897.79599.75
3766954-766954103.281105.32
4738595-73859599.462101.33
5733880-73388098.827100.79
6719047-71904796.83098.71
60min1674372-67437290.81496.963.4993.2699.443.40
2727578-72757897.979100.48
3721152-72115297.11399.72
4751327-751327101.177103.60
5724800-72480097.604100.12
6720825-72082597.06999.49
极限1713845-71384596.12997.373.0299.08100.392.96
2699228-69922894.16197.20
3733867-73386798.825101.97
4723266-72326697.398100.39
5760145-760145102.364105.42
6707871-70787195.32598.28
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