辅酶Q10片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号2306201对照品来源原料药对照品使用方法直接使用
对照品含量(%)99.5对照品水分(%)0对照品稀释倍数10000
标示量(mg)10供试品稀释倍数10系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.952583342592582579212597062579672586370.32
29.982557992551792554890.18
单位质量响应值RSD%判断
25993.6725600.101.08数据可信
供试品溶液-2011707批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1161513-16151356.07049.5620.7856.0749.5620.78
2154326-15432653.57553.58
3178345-17834561.91361.91
4148831-14883151.66751.67
5103615-10361535.97035.97
6109945-10994538.16838.17
10min1190160-19016066.01559.5918.7566.1159.6718.75
2191224-19122466.38466.47
3206567-20656771.71171.81
4178327-17832761.90761.99
5129404-12940444.92344.98
6134226-13422646.59746.66
15min1202068-20206870.14965.6915.6770.3565.8715.68
2212231-21223173.67773.88
3221064-22106476.74476.97
4194315-19431567.45767.65
5151108-15110852.45852.59
6154531-15453153.64653.79
20min1210583-21058373.10569.1414.0773.4369.4314.09
2221060-22106076.74277.06
3228996-22899679.49779.85
4204952-20495271.15071.45
5162550-16255056.43056.65
6166792-16679257.90358.13
30min1220318-22031876.48573.6611.1076.9374.0711.13
2234747-23474781.49481.94
3234511-23451181.41281.89
4216998-21699875.33275.75
5184446-18444664.03164.35
6182129-18212963.22763.55
45min1225075-22507578.13677.328.3178.7177.858.35
2244843-24484384.99985.58
3239246-23924683.05583.67
4224972-22497278.10078.65
5199860-19986069.38269.81
6202329-20232970.24070.67
60min1227648-22764879.02979.556.0079.7380.216.05
2249326-24932686.55587.28
3238963-23896382.95783.71
4230057-23005779.86580.54
5216190-21619075.05175.59
6212735-21273573.85274.40
极限1261800-26180090.88588.425.9691.7289.216.01
2264464-26446491.81092.68
3267267-26726792.78393.68
4263972-26397291.63992.45
5233259-23325980.97781.64
6237406-23740682.41783.09
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