辅酶Q10片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号2306201对照品来源原料药对照品使用方法直接使用
对照品含量(%)99.5对照品水分(%)0对照品稀释倍数10000
标示量(mg)10供试品稀释倍数10系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.632480832470302473702488442487942480240.34
29.622474532478882476700.13
单位质量响应值RSD%判断
25755.3525745.320.03数据可信
供试品溶液-2011707批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1167853-16785358.37353.9411.3458.3753.9411.34
2175885-17588561.16661.17
3168796-16879658.70158.70
4138707-13870748.23748.24
5136551-13655147.48747.49
6142809-14280949.66449.66
10min1188367-18836765.50762.687.2365.6062.777.23
2197838-19783868.80168.90
3188926-18892665.70165.80
4169829-16982959.06059.14
5167837-16783758.36758.45
6168675-16867558.65958.74
15min1202645-20264570.47267.655.7970.6867.845.80
2208864-20886472.63572.85
3201170-20117069.95970.17
4183526-18352663.82364.00
5181386-18138663.07963.26
6189575-18957565.92766.11
20min1208275-20827572.43070.554.9072.7570.864.91
2217044-21704475.48075.82
3208422-20842272.48172.81
4192479-19247966.93767.22
5192761-19276167.03567.32
6198200-19820068.92769.22
30min1213147-21314774.12574.302.8674.5774.722.88
2225040-22504078.26078.72
3213921-21392174.39474.84
4211913-21191373.69574.09
5206798-20679871.91772.31
6211095-21109573.41173.82
45min1217581-21758175.66776.601.7276.2377.151.74
2226606-22660678.80579.40
3221641-22164177.07877.65
4219315-21931576.27076.79
5215716-21571675.01875.53
6220731-22073176.76277.29
60min1220928-22092876.83078.261.6577.5278.931.64
2228998-22899879.63780.36
3223235-22323577.63378.33
4227119-22711978.98379.63
5221173-22117376.91677.55
6228710-22871079.53780.19
极限1242953-24295384.49086.391.2585.3187.191.23
2248376-24837686.37687.23
3248423-24842386.39287.22
4251568-25156887.48688.26
5247889-24788986.20686.97
6251240-25124087.37288.16
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