辅酶Q10片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号2306201对照品来源原料药对照品使用方法直接使用
对照品含量(%)99.5对照品水分(%)0对照品稀释倍数10000
标示量(mg)10供试品稀释倍数10系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.632409922387362413462400302397412401690.44
29.622406902421772414340.44
单位质量响应值RSD%判断
24939.6725097.090.45数据可信
供试品溶液-24120501批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1144038-14403851.55752.933.4251.5652.933.43
2153596-15359654.97854.98
3145955-14595552.24352.24
10min1197788-19778870.79672.982.6970.8873.072.69
2208390-20839074.59174.68
3205485-20548573.55173.64
15min1176145-17614563.04962.342.3363.2562.552.32
2176867-17686763.30863.52
3169518-16951860.67760.89
20min1223281-22328179.92181.311.7880.2381.631.78
2231326-23132682.80183.12
3226908-22690881.22081.53
30min1185852-18585266.52466.670.7966.9767.120.80
2187869-18786967.24667.71
3185045-18504566.23566.68
45min1231955-23195583.02684.091.4483.5884.651.44
2238588-23858885.40085.97
3234276-23427683.85784.41
60min1193662-19366269.31969.241.7170.0169.941.71
2196610-19661070.37571.09
3190017-19001768.01568.71
极限1233520-23352083.58685.141.8084.3985.951.80
2242045-24204586.63887.47
3238013-23801385.19486.00
辅酶Q10片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号2306201对照品来源原料药对照品使用方法直接使用
对照品含量(%)99.5对照品水分(%)0对照品稀释倍数10000
标示量(mg)10供试品稀释倍数10系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.632384922395332404862413472399522399620.45
29.622424762408402416580.48
单位质量响应值RSD%判断
24918.1725120.370.58数据可信
供试品溶液-24120502批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1143747-14374751.45151.971.8851.4551.971.87
2148334-14833453.09353.09
3143510-14351051.36751.37
10min1154247-15424755.21053.676.7155.3053.766.71
2138447-13844749.55449.64
3157134-15713456.24356.33
15min1175693-17569362.88663.370.8263.0663.550.82
2178582-17858263.92064.09
3176896-17689663.31663.50
20min1185861-18586166.52564.526.5966.8164.806.57
2166619-16661959.63859.92
3188281-18828167.39167.68
30min1192965-19296569.06869.080.5669.4669.470.54
2194098-19409869.47369.85
3191948-19194868.70469.10
45min1202257-20225772.39470.027.0072.9070.526.97
2179864-17986464.37964.87
3204711-20471173.27273.78
60min1199500-19950071.40773.283.1572.0473.903.10
2211901-21190175.84676.45
3202758-20275872.57373.21
极限1213786-21378676.52073.565.1877.2774.305.15
2193517-19351769.26669.99
3209219-20921974.88675.64
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