非布司他片项目信息
介质体积(ml)900取样体积(ml)2补液体积(ml)2
对照品批号101278-202003对照品来源中检院对照品使用方法直接使用
对照品含量(%)100对照品水分(%)0对照品稀释倍数250
标示量(mg)40供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.043760199381251937926473806649380517537954380.56
210.173887669389019338889310.05
单位质量响应值RSD%判断
378031.67382392.430.82数据可信
供试品溶液-2024112521批-pH6.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min11771076-177107641.92536.3317.1741.9236.3317.18
21537820-153782036.40336.40
31879130-187913044.48244.48
41165277-116527727.58427.58
51345901-134590131.86031.86
61509923-150992335.74335.74
10min13427867-342786781.14476.977.2181.2477.057.21
23243003-324300376.76876.85
33505784-350578482.98883.09
43222280-322228076.27776.34
53278799-327879977.61577.69
62831068-283106867.01667.10
15min13859653-385965391.36590.233.8291.6490.483.82
23835584-383558490.79591.05
33850983-385098391.16091.44
43828045-382804590.61790.85
53963336-396333693.81994.06
63531959-353195983.60883.84
20min13987209-398720994.38494.292.9294.8694.742.91
24039951-403995195.63396.09
33963818-396381893.83194.32
43993049-399304994.52394.95
54133636-413363697.85198.30
63780926-378092689.50189.92
30min14064043-406404396.20397.781.7996.8998.441.78
24199153-419915399.401100.07
34086309-408630996.73097.42
44085362-408536296.70897.35
54245677-4245677100.503101.17
64102481-410248197.11397.73
45min14099714-409971497.04898.471.7797.9599.351.75
24274181-4274181101.177102.06
34101584-410158497.09298.00
44103959-410395997.14898.01
54219881-421988199.892100.78
64159360-415936098.45999.29
60min14115380-411538097.41898.861.9398.5399.961.91
24221735-422173599.936101.05
34089106-408910696.79697.92
44140972-414097298.02499.10
54309044-4309044102.003103.12
64182675-418267599.011100.06
极限14123610-412361097.61399.121.6498.95100.441.63
24283348-4283348101.394102.73
34143251-414325198.07899.42
44146868-414686898.16499.45
54264746-4264746100.954102.30
64162023-416202398.52299.79
非布司他片项目信息
介质体积(ml)900取样体积(ml)2补液体积(ml)2
对照品批号101278-202003对照品来源中检院对照品使用方法直接使用
对照品含量(%)100对照品水分(%)0对照品稀释倍数250
标示量(mg)40供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.043782529382049838154973821185382240138124220.45
210.173884272389925638917640.28
单位质量响应值RSD%判断
379723.31382670.990.55数据可信
供试品溶液-2024112621批-pH6.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min11831603-183160343.24437.9126.7143.2437.9126.71
21657899-165789939.14339.14
31823328-182332843.04943.05
41478469-147846934.90734.91
5815135-81513519.24519.25
62026512-202651247.84647.85
10min13370078-337007879.56873.769.2479.6673.859.25
22991129-299112970.62170.71
33392366-339236680.09480.19
43162420-316242074.66574.74
52617614-261761461.80261.85
63212118-321211875.83975.95
15min13859645-385964591.12787.754.0291.4088.004.04
23537179-353717983.51383.76
33840615-384061590.67890.95
43747277-374727788.47488.72
53524565-352456583.21683.40
63789585-378958589.47389.75
20min14028130-402813095.10593.191.8395.5893.631.87
23892621-389262191.90592.33
34005705-400570594.57595.05
43917601-391760192.49592.94
53845957-384595790.80491.17
63991604-399160494.24394.72
30min14175489-417548998.58496.991.1599.2797.641.19
24087239-408723996.50097.13
34134846-413484697.62498.31
44079015-407901596.30696.95
54042909-404290995.45496.02
64127377-412737797.44898.13
45min14232581-423258199.93298.390.95100.8499.250.98
24160514-416051498.23099.08
34192787-419278798.99299.89
44141641-414164197.78598.64
54123263-412326397.35198.13
64151890-415189098.02798.93
60min14240257-4240257100.11398.950.89101.24100.030.92
24177975-417797598.64399.71
34207492-420749299.340100.46
44160724-416072498.23599.31
54142266-414226697.80098.79
64216679-421667999.557100.67
极限14264902-4264902100.69599.061.17102.05100.371.21
24179458-417945898.67899.96
34227627-422762799.815101.16
44147987-414798797.93599.23
54138814-413881497.71898.93
64216261-421626199.547100.89
非布司他片项目信息
介质体积(ml)900取样体积(ml)2补液体积(ml)2
对照品批号101278-202003对照品来源中检院对照品使用方法直接使用
对照品含量(%)100对照品水分(%)0对照品稀释倍数250
标示量(mg)40供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.043820689383765138319123830389382140538284090.19
210.173926086393368839298870.14
单位质量响应值RSD%判断
381315.64386419.570.95数据可信
供试品溶液-2024112721批-pH6.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min11992514-199251446.71839.5013.0746.7239.5013.07
21635395-163539538.34438.34
31551433-155143336.37636.38
41914472-191447244.88844.89
51431038-143103833.55333.55
61583998-158399837.13937.14
10min13524201-352420182.63176.665.4382.7376.755.43
23061157-306115771.77471.86
33167035-316703574.25674.34
43445431-344543180.78480.88
53223067-322306775.57075.64
63197704-319770474.97575.06
15min13914654-391465491.78589.631.6392.0789.891.65
23777473-377747388.56988.81
33767216-376721688.32888.57
43872523-387252390.79891.08
53837773-383777389.98390.23
63767050-376705088.32588.57
20min14034979-403497994.60794.041.0395.1094.501.04
24044843-404484394.83895.28
33956540-395654092.76793.21
44032404-403240494.54695.03
54037233-403723394.65995.10
63959637-395963792.84093.29
30min14182348-418234898.06297.421.1598.7698.081.15
24211641-421164198.74999.40
34095879-409587996.03596.68
44152060-415206097.35298.04
54186317-418631798.15598.81
64100622-410062296.14696.80
45min14234871-423487199.29399.091.03100.2199.971.03
24293797-4293797100.675101.55
34196741-419674198.39999.26
44203755-420375598.56499.47
54253683-425368399.734100.61
64174431-417443197.87698.74
60min14278241-4278241100.31099.611.12101.45100.711.12
24325728-4325728101.424102.52
34205698-420569898.60999.69
44237557-423755799.356100.48
54242218-424221899.466100.56
64199927-419992798.47499.56
极限14204696-420469698.58699.611.1899.95100.941.17
24326604-4326604101.444102.77
34224937-422493799.060100.36
44237577-423757799.357100.70
54292526-4292526100.645101.96
64204760-420476098.58799.89
点击查看处理图标(自动生成)
　
原始图谱下载图谱(谢鑫慧 于 2024-12-12 13:09:19 完成)
生成报告数据部分下载报告(谢鑫慧 于 2024-12-12 13:09:39 完成)
Current page cost:66 ms