盐酸伐地那非片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号D23106010771对照品来源中检所对照品使用方法直接使用
对照品含量(%)90.12对照品水分(%)0对照品稀释倍数1000
标示量(mg)10供试品稀释倍数1系数0.9306
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
1 12.073764913770733754633771973772193766890.20
2 12.143775973772003773980.08
单位质量响应值RSD%判断
31208.7031087.150.28数据可信
供试品溶液-BXJVV51批-pH1.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1376866-37686691.32491.011.7791.3291.001.77
2386242-38624293.59693.60
3372919-37291990.36890.37
4379068-37906891.85891.86
5368472-36847289.29089.29
6369728-36972889.59589.59
10min1402211-40221197.46697.650.4097.6297.800.40
2404903-40490398.11898.27
3400865-40086597.14097.29
4404549-40454998.03398.19
5403469-40346997.77197.92
6401877-40187797.38597.53
15min1405595-40559598.28698.360.2898.6098.680.28
2404104-40410497.92598.24
3405760-40576098.32698.64
4407473-40747398.74199.06
5406013-40601398.38798.70
6406510-40651098.50898.82
20min1409575-40957599.25198.630.6099.7399.110.60
2403823-40382397.85798.34
3406441-40644198.49198.97
4409808-40980899.30799.79
5404871-40487198.11198.59
6407510-40751098.75099.23
30min1407677-40767798.79198.770.5899.4399.410.57
2403253-40325397.71998.36
3407553-40755398.76199.40
4408721-40872199.04499.69
5408273-40827398.93599.57
6410157-41015799.392100.03
45min1408802-40880299.06398.760.5199.8799.560.50
2403642-40364297.81398.62
3409134-40913499.14499.95
4407512-40751298.75199.56
5408816-40881699.06799.87
6407270-40727098.69299.50
60min1407068-40706898.64398.860.6099.6299.830.59
2403548-40354897.79098.76
3409716-40971699.285100.26
4408099-40809998.89399.87
5409236-40923699.168100.14
6410055-41005599.367100.34
极限1407989-40798998.86698.941.27100.00100.081.26
2401400-40140097.26998.40
3406471-40647198.49899.63
4408310-40831098.944100.09
5417412-417412101.150102.28
6408299-40829998.941100.08
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