替米沙坦氨氯地平片项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号22AD265对照品来源工作对照品对照品使用方法直接使用
对照品含量(%)99.7对照品水分(%)0对照品稀释倍数10000
标示量(mg)5供试品稀释倍数5系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
1 15.282976829797297162973229663297350.18
2 15.212962529799297120.42
单位质量响应值RSD%判断
1946.011953.450.27数据可信
供试品溶液-24101501批-氨氯地平-水
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min122167-2216773.55478.224.1273.5578.224.12
224408-2440880.99080.99
323567-2356778.20078.20
422657-2265775.18075.18
524102-2410279.97579.97
624533-2453381.40581.40
10min126837-2683789.05087.312.2489.4687.742.24
226630-2663088.36388.81
325902-2590285.94886.38
425384-2538484.22984.65
526235-2623587.05287.50
626882-2688289.19989.65
15min128124-2812493.32189.103.2194.2290.023.18
226615-2661588.31389.25
326155-2615586.78787.70
425872-2587285.84886.73
526748-2674888.75589.68
627604-2760491.59592.54
20min128288-2828893.86589.033.6995.2990.453.65
225779-2577985.53986.97
326430-2643087.70089.09
425836-2583685.72987.09
527249-2724990.41791.84
627410-2741090.95192.41
30min126819-2681988.99088.972.5490.9390.882.52
227790-2779092.21294.12
326356-2635687.45489.34
426062-2606286.47888.32
526392-2639287.57389.50
627453-2745391.09493.06
45min125043-2504383.09784.091.5685.5386.491.53
225836-2583685.72988.15
324941-2494182.75985.13
425417-2541784.33886.66
525043-2504383.09785.51
625771-2577185.51387.98
60min123781-2378178.91083.114.9381.8185.984.76
225082-2508283.22786.12
325602-2560284.95287.78
425609-2560984.97587.76
523466-2346677.86480.74
626741-2674188.73191.67
极限125042-2504283.09484.715.5286.4388.045.34
226236-2623687.05690.41
326189-2618986.90090.20
425793-2579385.58688.85
522952-2295276.15979.46
626954-2695489.43892.87
替米沙坦氨氯地平片项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号100320240115对照品来源工作对照品对照品使用方法直接使用
对照品含量(%)100对照品水分(%)0对照品稀释倍数625
标示量(mg)80供试品稀释倍数5系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
1 10.898700438703038697968696318697918699130.04
211.068674998670638672810.04
单位质量响应值RSD%判断
79881.8278416.001.31数据可信
供试品溶液-24101501批-替米沙坦-水
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1435057-43505749.47452.335.0449.4752.335.04
2476556-47655654.19454.19
3457528-45752852.03052.03
4458330-45833052.12152.12
5495910-49591056.39556.39
6437830-43783049.79049.79
10min1722406-72240682.15284.943.1582.4385.233.15
2775401-77540188.17888.48
3740236-74023684.17984.47
4729705-72970582.98283.27
5776892-77689288.34888.66
6736831-73683183.79284.07
15min1862302-86230298.06198.561.5798.7999.321.58
2868646-86864698.78299.57
3858128-85812897.58698.34
4867720-86772098.67799.43
5891393-891393101.369102.17
6852196-85219696.91197.65
20min1918266-918266104.425101.801.81105.70103.111.79
2885529-885529100.702102.04
3886763-886763100.842102.14
4886127-886127100.770102.07
5913280-913280103.858105.23
6881224-881224100.212101.49
30min1900272-900272102.378102.600.82104.23104.480.80
2914380-914380103.983105.88
3892750-892750101.523103.38
4903803-903803102.780104.64
5897750-897750102.092104.04
6904356-904356102.843104.68
45min1844672-84467296.05697.691.7098.48100.131.68
2862420-86242098.074100.55
3839714-83971495.49297.91
4860330-86033097.836100.27
5878131-87813199.861102.37
6868876-86887698.808101.22
60min1831932-83193294.60798.582.6597.57101.572.58
2900603-900603102.416105.44
3879759-879759100.046103.00
4867422-86742298.643101.62
5857628-85762897.529100.60
6863706-86370698.220101.18
极限1847399-84739996.36699.431.7199.85102.971.68
2891758-891758101.410105.00
3881539-881539100.248103.76
4878818-87881899.939103.46
5875392-87539299.549103.16
6871222-87122299.075102.58
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