贝派度酸片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号BEMA-231010D对照品来源自制对照品使用方法直接使用
对照品含量(%)99.72对照品水分(%)0对照品稀释倍数50
标示量(mg)180供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.073029843028993029453030473030713029890.03
210.023037713038663038180.03
单位质量响应值RSD%判断
30088.2830321.160.55数据可信
供试品溶液-24122501批-pH6.6
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1107213-10721335.39732.9511.3135.4032.9511.31
2105498-10549834.83034.83
397986-9798632.35032.35
498964-9896432.67332.67
5110206-11020636.38536.38
678916-7891626.05426.05
10min1223745-22374573.87072.962.3373.9373.022.34
2225151-22515174.33474.39
3219393-21939372.43372.49
4221970-22197073.28473.34
5224304-22430474.05474.12
6211364-21136469.78269.83
15min1263988-26398887.15687.521.1687.3487.691.17
2269888-26988889.10489.29
3263514-26351487.00087.17
4265572-26557287.67987.86
5266579-26657988.01288.20
6260913-26091386.14186.30
20min1281658-28165892.99093.570.9493.3293.890.95
2287018-28701894.76095.09
3283334-28333493.54393.86
4284159-28415993.81694.14
5284965-28496594.08294.41
6279382-27938292.23992.54
30min1293876-29387697.02497.930.8797.5198.410.87
2300410-30041099.18199.67
3297353-29735398.17298.65
4297152-29715298.10598.58
5297396-29739698.18698.67
6293499-29349996.89997.36
45min1299445-29944598.86299.950.8499.51100.590.84
2306330-306330101.135101.79
3304177-304177100.425101.06
4303328-303328100.144100.79
5302756-30275699.955100.61
6300330-30033099.15599.77
60min1300735-30073599.288100.530.99100.10101.340.98
2307959-307959101.673102.50
3307779-307779101.614102.42
4304849-304849100.647101.46
5303776-303776100.292101.11
6301851-30185199.657100.44
极限1305544-305544100.876101.760.66101.85102.740.66
2310514-310514102.517103.51
3310441-310441102.493103.47
4308200-308200101.753102.73
5308150-308150101.736102.72
6306543-306543101.206102.16
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