美阿沙坦钾片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号D211-4R701-2402002对照品来源自制工作对照品对照品使用方法直接使用
对照品含量(%)99.5对照品水分(%)0对照品稀释倍数1000
标示量(mg)80供试品稀释倍数5系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
118.032084952075442084212074362079132079620.24
218.072075182071092073140.14
单位质量响应值RSD%判断
11534.2211472.830.38数据可信
供试品溶液-2025010221批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min113647-136476.6407.488.826.647.488.82
215792-157927.6837.68
315630-156307.6057.60
414973-149737.2857.28
514554-145547.0817.08
617638-176388.5828.58
10min139670-3967019.30121.936.5419.3722.026.55
245710-4571022.24022.33
347205-4720522.96723.05
444331-4433121.56921.65
545574-4557422.17422.25
647982-4798223.34523.44
15min157433-5743327.94329.083.0328.2329.413.05
261075-6107529.71530.05
362207-6220730.26630.61
458495-5849528.46028.78
560607-6060729.48829.81
658793-5879328.60528.96
20min167618-6761832.89934.252.0333.5034.902.07
271610-7161034.84135.50
370871-7087134.48235.16
470286-7028634.19734.83
570793-7079334.44435.10
671174-7117434.62935.30
30min180137-8013738.99039.771.5939.9540.801.62
281018-8101839.41840.47
384000-8400040.86941.93
481399-8139939.60440.62
582059-8205939.92540.96
681779-8177939.78940.85
45min188221-8822142.92344.181.6544.3245.651.68
291449-9144944.49445.98
392364-9236444.93946.45
491185-9118544.36545.82
589951-8995143.76545.24
691664-9166444.59846.10
60min192328-9232844.92146.162.4946.8048.122.42
293885-9388545.67947.66
396867-9686747.13049.14
497734-9773447.55149.50
596145-9614546.77848.74
692312-9231244.91346.91
极限1101292-10129249.28350.091.3251.6652.561.33
2102365-10236549.80552.29
3104422-10442250.80553.34
4104550-10455050.86853.35
5103230-10323050.22552.71
6101841-10184149.55052.04
美阿沙坦钾片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号D211-4R701-2402002对照品来源自制工作对照品对照品使用方法直接使用
对照品含量(%)99.5对照品水分(%)0对照品稀释倍数1000
标示量(mg)80供试品稀释倍数5系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
118.032077702084102079402070872080242078460.24
218.072062282072992067640.37
单位质量响应值RSD%判断
11527.7911442.390.53数据可信
供试品溶液-2025010221批
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min117363-173638.4618.5121.348.468.5121.32
220035-200359.7649.76
320696-2069610.08610.09
419924-199249.7099.71
510826-108265.2765.28
615958-159587.7777.78
10min146183-4618322.50622.957.0722.6023.047.13
248058-4805823.42023.53
349912-4991224.32324.44
449788-4978824.26324.37
540927-4092719.94520.00
647682-4768223.23723.32
15min161178-6117829.81330.303.8330.1630.653.90
262520-6252030.46730.84
364741-6474131.55031.93
463239-6323930.81831.20
557949-5794928.24028.52
663463-6346330.92731.27
20min170697-7069734.45234.852.9035.1335.542.97
272908-7290835.53036.24
372601-7260135.38036.11
471864-7186435.02135.74
567738-6773833.01033.60
673311-7331135.72636.41
30min184069-8406940.96940.132.2442.0341.212.30
281585-8158539.75840.86
383364-8336440.62541.75
483130-8313040.51141.62
578978-7897838.48839.45
683020-8302040.45841.54
45min191462-9146244.57244.981.6446.0846.491.71
291554-9155444.61646.16
393921-9392145.77047.35
493255-9325545.44547.00
590047-9004743.88245.27
693502-9350245.56647.10
60min195767-9576746.66946.631.5048.6848.651.54
293975-9397545.79647.84
397752-9775247.63749.72
496683-9668347.11649.18
594257-9425745.93447.81
695659-9565946.61748.66
极限1104621-10462150.98450.201.1753.5152.741.14
2103643-10364350.50853.06
3101656-10165649.53952.15
4102536-10253649.96852.56
5101787-10178749.60351.99
6103797-10379750.58353.14
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