辅酶Q10片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号140611-202107对照品来源中检所对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数500
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.962685262680112681702681982675352680880.14
29.942684862690162687510.14
单位质量响应值RSD%判断
26916.4727037.320.32数据可信
供试品溶液-25021901批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1155464-15546457.51456.412.8957.5156.402.89
2156676-15667657.96257.96
3146949-14694954.36354.36
4146896-14689654.34454.34
5154976-15497657.33357.33
6153856-15385656.91956.92
10min1190128-19012870.33770.232.1070.5170.402.10
2193927-19392771.74371.92
3185362-18536268.57468.74
4185867-18586768.76168.92
5194875-19487572.09472.27
6188915-18891569.88970.06
15min1204571-20457175.68176.572.2276.0676.952.22
2212059-21205978.45178.84
3202535-20253574.92775.30
4203852-20385275.41575.78
5213409-21340978.95079.34
6205369-20536975.97676.36
20min1212922-21292278.77080.292.4679.3880.902.46
2222224-22222482.21182.84
3212016-21201678.43579.03
4215252-21525279.63280.23
5225085-22508583.27083.89
6214693-21469379.42580.03
30min1219714-21971481.28383.552.5082.1384.402.50
2232186-23218685.89786.77
3221573-22157381.97182.80
4224450-22445083.03583.87
5233376-23337686.33787.21
6223706-22370682.76083.61
45min1224127-22412782.91585.592.8684.0186.702.84
2237488-23748887.85888.99
3227105-22710584.01785.09
4232101-23210185.86586.95
5240700-24070089.04690.18
6226677-22667783.85984.95
60min1226896-22689683.94086.312.6885.2887.672.67
2238556-23855688.25389.65
3228504-22850484.53585.86
4233825-23382586.50387.84
5242657-24265789.77091.17
6229419-22941984.87386.22
极限1256337-25633794.83196.491.6296.4298.101.63
2265597-26559798.25799.91
3258291-25829195.55497.13
4261536-26153696.75598.36
5265938-26593898.383100.05
6257182-25718295.14496.75
辅酶Q10片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号140611-202107对照品来源中检所对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数500
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.962693522690812690622687492692102690910.09
29.942681652676922679280.13
单位质量响应值RSD%判断
27017.1726954.530.17数据可信
供试品溶液-25021902批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1159473-15947358.97757.752.6358.9857.752.63
2160945-16094559.52159.52
3153189-15318956.65356.65
4159105-15910558.84158.84
5152313-15231356.32956.33
6151911-15191156.18056.18
10min1188193-18819369.59868.512.1869.7868.692.19
2189059-18905969.91970.10
3180312-18031266.68466.85
4189060-18906069.91970.10
5183788-18378867.96968.14
6181129-18112966.98667.15
15min1205178-20517875.88075.271.8476.2775.651.85
2207746-20774676.82977.22
3199916-19991673.93474.30
4207537-20753776.75277.14
5200922-20092274.30674.68
6199842-19984273.90674.28
20min1217353-21735380.38279.001.6381.0079.611.64
2214296-21429679.25279.87
3209268-20926877.39277.98
4217842-21784280.56381.18
5211747-21174778.30978.90
6211227-21122778.11778.71
30min1225625-22562583.44283.071.5884.3083.911.58
2227307-22730784.06484.92
3219598-21959881.21382.04
4229312-22931284.80585.66
5223873-22387382.79483.62
6222020-22202082.10882.93
45min1233597-23359786.39085.371.5487.4986.461.54
2232561-23256186.00787.12
3225083-22508383.24184.31
4234766-23476686.82287.93
5229762-22976284.97186.05
6229345-22934584.81785.89
60min1234654-23465486.78185.941.3588.1487.281.36
2233631-23363186.40287.77
3228155-22815584.37785.69
4236331-23633187.40188.77
5232068-23206885.82487.16
6229439-22943984.85286.18
极限1262730-26273097.16496.921.8698.7998.531.86
2264643-26464397.87199.50
3254876-25487694.25995.83
4269241-26924199.572101.21
5259255-25925595.87997.47
6261683-26168396.77798.36
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