多替诺雷片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号D241101对照品来源工作对照品对照品使用方法直接使用
对照品含量(%)99.69对照品水分(%)0对照品稀释倍数5000
标示量(mg)2供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.004762847504476524750547418475410.21
29.994763347440475360.29
单位质量响应值RSD%判断
4754.104758.360.07数据可信
供试品溶液-H046R批-水
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min112771-1277124.09129.5611.1224.0929.5611.13
216622-1662231.35631.36
316453-1645331.03731.04
414386-1438627.13827.14
516343-1634330.82930.83
617446-1744632.91032.91
10min121468-2146840.49748.468.8240.5448.508.82
226574-2657450.12950.18
326844-2684450.63850.69
424832-2483246.84346.89
526766-2676650.49150.54
627639-2763952.13852.19
15min127242-2724251.38959.727.3351.5059.857.34
232721-3272161.72561.86
333014-3301462.27762.41
430965-3096558.41258.54
532558-3255861.41761.55
633436-3343663.07363.22
20min130479-3047957.49566.217.0757.6966.447.08
235786-3578667.50667.75
336400-3640068.66568.90
434212-3421264.53764.76
536518-3651868.88769.13
637209-3720970.19170.44
30min135026-3502666.07374.456.0666.3674.796.07
239652-3965274.79975.15
340692-4069276.76177.12
438806-3880673.20373.53
541237-4123777.78978.14
641391-4139178.08078.44
45min139036-3903673.63781.294.9374.0481.764.94
243464-4346481.99082.47
343817-4381782.65683.14
442806-4280680.74981.20
544745-4474584.40784.89
644696-4469684.31484.81
60min142124-4212479.46285.593.9679.9886.193.98
245754-4575486.31086.92
345835-4583586.46387.08
444721-4472184.36184.95
546686-4668688.06888.69
647120-4712088.88789.52
90min144920-4492084.73789.403.2585.3990.143.27
246965-4696588.59489.35
347483-4748389.57190.34
446981-4698188.62489.35
548705-4870591.87792.65
649298-4929892.99593.78
120min146545-4654587.80291.762.5388.6092.652.55
248301-4830191.11592.02
348739-4873991.94192.85
448557-4855791.59792.47
549758-4975893.86394.79
649965-4996594.25395.19
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
极限146956-4695688.57792.502.6789.5293.542.69
248426-4842691.35092.41
349394-4939493.17694.24
448747-4874791.95692.98
550060-5006094.43395.51
650634-5063495.51596.61
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