非奈利酮片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号D231201对照品来源自制对照品使用方法直接使用
对照品含量(%)99.92对照品水分(%)0对照品稀释倍数1000
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.191900231901001899831900741901281900620.04
211.171922931921971922450.04
单位质量响应值RSD%判断
16984.9917210.830.94数据可信
供试品溶液-25031101批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min132332-3233217.00623.5118.0817.0123.5118.08
249420-4942025.99425.99
351901-5190127.29927.30
441413-4141321.78221.78
540200-4020021.14421.14
652962-5296227.85727.86
10min190622-9062247.66649.833.1747.6949.873.18
297624-9762451.34851.39
397425-9742551.24451.29
491468-9146848.11148.15
595316-9531650.13450.17
695935-9593550.46050.51
15min1114372-11437260.15860.521.3860.2760.651.39
2117379-11737961.73961.87
3116388-11638861.21861.35
4113680-11368059.79459.91
5113336-11333659.61359.73
6115242-11524260.61560.75
20min1127162-12716266.88566.970.8067.0967.200.81
2128601-12860167.64267.87
3127676-12767667.15567.39
4126347-12634766.45666.67
5128175-12817567.41867.64
6126017-12601766.28366.51
30min1141977-14197774.67774.310.7375.0074.650.73
2141721-14172174.54374.89
3141375-14137574.36174.71
4141151-14115174.24374.57
5142154-14215474.77075.10
6139322-13932273.28173.62
45min1153298-15329880.63280.300.8281.0880.760.81
2153256-15325680.61081.08
3152110-15211080.00780.48
4153201-15320180.58181.03
5153759-15375980.87481.33
6150400-15040079.10879.57
60min1160451-16045184.39483.960.9084.9784.550.88
2159722-15972284.01184.61
3159113-15911383.69184.29
4160551-16055184.44785.03
5160859-16085984.60985.20
6157025-15702582.59283.19
极限1164177-16417786.35485.700.9887.0786.440.97
2162776-16277685.61786.36
3162177-16217785.30286.04
4164585-16458586.56987.29
5163687-16368786.09686.83
6160240-16024084.28385.02
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