非奈利酮片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号D231201对照品来源自制对照品使用方法直接使用
对照品含量(%)99.92对照品水分(%)0对照品稀释倍数1000
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.191900941900281900461899441901051900430.04
211.171917031914461915740.10
单位质量响应值RSD%判断
16983.2917150.760.70数据可信
供试品溶液-BXK3152批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min149262-4926225.95723.4711.7425.9623.4711.74
238530-3853020.30220.30
344197-4419723.28823.29
447171-4717124.85624.86
549967-4996726.32926.33
638085-3808520.06820.07
10min1105283-10528355.47654.333.3255.5254.373.32
298905-9890552.11552.15
3103016-10301654.28254.32
4102965-10296554.25554.30
5108328-10832857.08157.12
6100178-10017852.78652.82
15min1130588-13058868.81068.001.9868.9568.141.99
2125788-12578866.28166.40
3128691-12869167.81067.94
4128049-12804967.47267.60
5133220-13322070.19770.34
6128015-12801567.45467.58
20min1145471-14547176.65276.161.4276.9076.401.43
2141635-14163574.63174.86
3145093-14509376.45376.70
4143110-14311075.40875.65
5147577-14757777.76278.02
6144311-14431176.04176.27
30min1162625-16262585.69185.390.9886.0785.760.99
2159785-15978584.19484.55
3162563-16256385.65886.03
4160819-16081984.73985.11
5164356-16435686.60386.99
6162233-16223385.48485.84
45min1175844-17584492.65692.460.9193.1892.970.91
2173795-17379591.57792.07
3175201-17520192.31892.83
4173672-17367291.51292.02
5177679-17767993.62394.15
6176638-17663893.07593.58
60min1181217-18121795.48795.680.8896.1696.340.87
2179797-17979794.73995.39
3183321-18332196.59697.26
4179689-17968994.68295.35
5182603-18260396.21896.90
6182831-18283196.33897.00
极限1182951-18295196.40196.740.6997.2497.560.69
2182617-18261796.22597.03
3183537-18353796.71097.54
4182212-18221296.01296.83
5185232-18523297.60398.45
6184972-18497297.46698.28
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