玛巴洛沙韦干混悬剂项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号DQTL-4125-250109对照品来源自制对照品使用方法直接使用
对照品含量(%)99.77对照品水分(%)0对照品稀释倍数2500
标示量(mg)40供试品稀释倍数10系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.219947799777994219944999327994900.18
211.279953199577995540.04
单位质量响应值RSD%判断
8875.118833.540.34数据可信
供试品溶液-B2021B01批-40mg-pH6.8(内含0.16%CTAB)
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min151810-5181052.54259.1813.3552.5459.1813.35
254631-5463155.40255.40
367354-6735468.30568.31
467410-6741068.36268.36
559613-5961360.45560.45
649307-4930750.00350.00
10min173008-7300874.03977.388.0574.3377.718.07
272097-7209773.11573.42
382040-8204083.19883.58
483407-8340784.58584.96
579193-7919380.31180.65
668059-6805969.02069.30
15min182078-8207883.23787.174.9883.9487.935.03
286075-8607587.29088.00
388708-8870889.96190.80
490202-9020291.47692.33
589125-8912590.38391.17
679560-7956080.68381.34
20min193391-9339194.71093.722.0095.8894.972.03
291636-9163692.93094.13
391775-9177593.07194.41
493765-9376595.08996.45
594490-9449095.82497.11
689445-8944590.70891.82
30min194031-9403195.35994.591.7597.0596.361.74
290849-9084992.13293.85
392146-9214693.44795.31
494048-9404895.37697.26
595489-9548996.83798.65
693098-9309894.41396.03
45min195855-9585597.20896.191.5199.4398.481.55
294082-9408295.41097.64
394204-9420495.53497.91
495797-9579797.15099.57
596489-9648997.851100.21
692706-9270694.01596.15
60min191988-9198893.28793.712.5596.0596.532.50
290280-9028091.55594.31
389166-8916690.42593.33
494703-9470396.04099.00
594885-9488596.22599.12
693387-9338794.70697.37
极限191748-9174893.04394.802.3496.3298.152.32
291878-9187893.17596.44
392730-9273094.03997.45
493547-9354794.86898.36
597677-9767799.056102.49
693315-9331594.63397.82
玛巴洛沙韦干混悬剂项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号DQTL-4125-250109对照品来源自制对照品使用方法直接使用
对照品含量(%)99.77对照品水分(%)0对照品稀释倍数2500
标示量(mg)40供试品稀释倍数10系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.219905899302992279932499052991930.14
211.271007231006251006740.07
单位质量响应值RSD%判断
8848.628932.920.68数据可信
供试品溶液-B2021B01批-40mg-pH6.8(内含0.16%CTAB)
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min181314-8131482.12684.511.5182.1384.511.51
284180-8418085.02085.02
384401-8440185.24385.24
483179-8317984.00984.01
584606-8460685.45085.45
684348-8434885.19085.19
10min191182-9118292.09293.941.0792.5594.411.07
293062-9306293.99194.46
393737-9373794.67395.15
493434-9343494.36794.83
593906-9390694.84395.32
692766-9276693.69294.17
15min193852-9385294.78995.731.3095.7696.721.29
295033-9503395.98196.98
395973-9597396.93197.93
496122-9612297.08198.07
592935-9293593.86394.86
694786-9478695.73296.73
20min194022-9402294.96095.411.1596.4596.931.14
296122-9612297.08198.61
394737-9473795.68397.22
494433-9443395.37596.91
592804-9280493.73095.25
694669-9466995.61497.14
30min195354-9535496.30696.570.6098.3398.620.59
296650-9665097.61599.68
395132-9513296.08198.15
495639-9563996.59498.65
595750-9575096.70698.75
695166-9516696.11698.17
45min193310-9331094.24194.651.2696.8097.241.24
292748-9274893.67496.28
395115-9511596.06498.67
494855-9485595.80298.40
592155-9215593.07595.66
694122-9412295.06197.65
60min193697-9369794.63293.881.4097.7196.991.35
294640-9464095.58598.71
390976-9097691.88495.02
493422-9342294.35497.48
592980-9298093.90897.01
691991-9199192.90996.03
极限193112-9311294.04194.200.2397.6597.840.23
293009-9300993.93797.60
393475-9347594.40898.06
493537-9353794.47198.12
593185-9318594.11597.73
693311-9331194.24297.88
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