布洛芬混悬液项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100179-202308对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数50
标示量(mg)200供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.662737057274254227436772738942273784027400120.11
210.732736774275110927439420.37
单位质量响应值RSD%判断
257036.77255726.190.37数据可信
供试品溶液-25052501批-pH7.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min12787784-278778497.76595.592.6597.7695.592.65
22679569-267956993.97093.97
32684475-268447594.14294.14
42624715-262471592.04692.05
52787493-278749397.75597.75
62790946-279094697.87697.88
10min12862560-2862560100.387100.031.38100.55100.191.37
22921544-2921544102.456102.61
32860546-2860546100.317100.47
42831079-283107999.28399.44
52815703-281570398.74498.91
62822389-282238998.97999.14
15min12874831-2874831100.818100.181.60101.15100.501.59
22931619-2931619102.809103.14
32872475-2872475100.735101.06
42822884-282288498.99699.31
52811605-281160598.60098.93
62825706-282570699.09599.42
20min12870648-2870648100.671100.131.65101.17100.621.65
22932309-2932309102.833103.33
32874074-2874074100.791101.28
42818818-281881898.85399.34
52803682-280368298.32398.81
62831560-283156099.30099.79
30min12871916-2871916100.71599.951.72101.38100.601.71
22926631-2926631102.634103.30
32870310-2870310100.659101.32
42811153-281115398.58599.23
52795292-279529298.02898.68
62824600-282460099.05699.71
极限12876085-2876085100.86299.891.87101.70100.721.87
22932944-2932944102.856103.70
32864338-2864338100.450101.28
42816824-281682498.78399.60
52788166-278816697.77898.60
62811592-281159298.60099.42
布洛芬混悬液项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100179-202308对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数50
标示量(mg)200供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.662742870273864127492082743295274216127432350.14
210.732727716272742427275700.01
单位质量响应值RSD%判断
257339.12254200.370.87数据可信
供试品溶液-25052601批-pH7.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min12556984-255698489.88887.944.1789.8987.944.17
22452302-245230286.20886.21
32578712-257871290.65290.65
42388082-238808283.95183.95
52395208-239520884.20184.20
62638348-263834892.74992.75
10min12945712-2945712103.554100.302.75103.70100.452.75
22926277-2926277102.870103.01
32895691-2895691101.795101.95
42782735-278273597.82497.96
52766276-276627697.24697.39
62803001-280300198.53798.69
15min12954693-2954693103.869100.572.71104.19100.882.70
22928855-2928855102.961103.28
32905496-2905496102.140102.46
42787347-278734797.98698.29
52786700-278670097.96498.27
62801544-280154498.48698.80
20min12959106-2959106104.025100.382.77104.52100.862.77
22915525-2915525102.492102.98
32901587-2901587102.002102.49
42782677-278267797.82298.29
52783051-278305197.83598.30
62791268-279126898.12498.61
30min12959026-2959026104.022100.202.85104.69100.852.85
22917236-2917236102.553103.21
32888081-2888081101.528102.19
42773389-277338997.49698.13
52780741-278074197.75498.38
62783549-278354997.85398.50
极限12947598-2947598103.620100.182.66104.46100.992.65
22916598-2916598102.530103.36
32883808-2883808101.377102.21
42776199-277619997.59598.39
52790128-279012898.08498.88
62783423-278342397.84998.66
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