他克莫司颗粒项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号130550-202401对照品来源中检所对照品使用方法直接使用
对照品含量(%)97.9对照品水分(%)0对照品稀释倍数17500
标示量(mg)1供试品稀释倍数1.4系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
1 13.921529861531671530921526341528731529500.14
2 13.901526421523741525080.13
单位质量响应值RSD%判断
10987.7910971.800.11数据可信
供试品溶液-2025052021批-含0.005%羟丙基纤维素的pH4.5溶液
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min174189-7418947.62846.303.2947.6346.303.29
271630-7163045.98545.99
374879-7487948.07148.07
468511-6851143.98343.98
572896-7289646.79846.80
670603-7060345.32645.33
10min1101710-10171065.29663.803.1765.8264.313.16
295518-9551861.32161.83
399813-9981364.07864.61
496227-9622761.77662.26
5103725-10372566.58967.11
699244-9924463.71364.22
15min1114696-11469673.63272.993.9074.8974.213.87
2109668-10966870.40571.60
3121370-12137077.91779.16
4110587-11058770.99572.17
5115249-11524973.98875.25
6110564-11056470.98072.19
20min1124367-12436779.84178.592.5381.9180.622.54
2118717-11871776.21478.19
3126408-12640881.15183.26
4118952-11895276.36578.33
5123940-12394079.56781.65
6122133-12213378.40780.41
30min1133905-13390585.96485.632.4088.9288.542.41
2130236-13023683.60986.43
3137625-13762588.35291.37
4129115-12911582.88985.70
5135431-13543186.94489.91
6134040-13404086.05188.92
45min1142074-14207491.20990.722.6795.1294.582.67
2138305-13830588.78992.54
3146951-14695194.34098.33
4136643-13664387.72291.46
5143805-14380592.32096.25
6140101-14010189.94293.77
60min1144606-14460692.83492.971.9197.7697.841.94
2142408-14240891.42396.16
3149657-14965796.077101.12
4143239-14323991.95796.66
5146236-14623693.88198.84
6142748-14274891.64196.47
90min1146542-14654294.07794.242.35100.04100.142.35
2142116-14211691.23696.99
3151296-15129697.129103.24
4143847-14384792.34798.08
5149651-14965196.073102.07
6147348-14734894.594100.44
极限1143691-14369192.24792.402.9199.2599.342.87
2138691-13869189.03795.80
3151142-15114297.030104.22
4141569-14156990.88497.64
5145277-14527793.265100.33
6143198-14319891.93098.83
他克莫司颗粒项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号130550-202401对照品来源中检所对照品使用方法直接使用
对照品含量(%)97.9对照品水分(%)0对照品稀释倍数17500
标示量(mg)1供试品稀释倍数1.4系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
1 13.921526411527361526031520731520261524160.23
2 13.901521011519301520160.08
单位质量响应值RSD%判断
10949.4310936.400.09数据可信
供试品溶液-2025052021批
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min168676-6867644.23744.623.9744.2444.623.97
266004-6600442.51642.52
370933-7093345.69145.69
471015-7101545.74445.74
566286-6628642.69842.70
672746-7274646.85946.86
10min199917-9991764.36162.184.3764.8562.674.35
288579-8857957.05857.53
398199-9819963.25463.76
499807-9980764.29064.80
595896-9589661.77162.25
696744-9674462.31762.84
15min1113740-11374073.26572.233.4374.4773.423.43
2105171-10517167.74568.85
3116722-11672275.18676.40
4111384-11138471.74772.97
5112859-11285972.69773.86
6112906-11290672.72873.94
20min1121267-12126778.11379.553.6580.1381.543.62
2117732-11773275.83677.70
3131272-13127284.55886.60
4123207-12320779.36381.38
5122647-12264779.00280.97
6124879-12487980.44082.46
30min1133949-13394986.28286.894.4689.1789.774.41
2124203-12420380.00582.71
3142454-14245491.76194.75
4135446-13544687.24790.15
5137568-13756888.61391.46
6135748-13574887.44190.36
45min1144919-14491993.34992.394.5897.2096.234.53
2131120-13112084.46088.05
3149227-14922796.124100.13
4142250-14225091.62995.50
5144662-14466293.18397.01
6148411-14841195.59899.48
60min1144418-14441893.02694.614.3497.9199.484.29
2136206-13620687.73692.27
3153835-15383599.092104.16
4145340-14534093.62098.51
5151716-15171697.727102.59
6149757-14975796.465101.41
90min1145781-14578193.90496.043.3199.82101.963.30
2141076-14107690.87396.38
3151932-15193297.866104.04
4149560-14956096.338102.27
5154766-15476699.691105.64
6151494-15149497.584103.60
极限1142112-14211291.54093.583.9798.50100.563.94
2135434-13543487.23993.75
3150855-15085597.172104.43
4145454-14545493.693100.69
5149850-14985096.525103.58
6147937-14793795.293102.40
点击查看处理图标(人工保存)
　
原始图谱下载图谱(姜进硙 于 2025-06-16 15:50:17 完成)
生成报告数据部分(等待生成报告)
Current page cost:73 ms