枸橼酸西地那非片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号420012-202204对照品来源中检院对照品使用方法直接使用
对照品含量(%)98.8对照品水分(%)0对照品稀释倍数125
标示量(mg)100供试品稀释倍数1系数0.7118
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
117.322336062344032342192339132334792339240.17
217.352330852337072333960.19
单位质量响应值RSD%判断
13506.0013452.220.29数据可信
供试品溶液-22030701批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1189052-18905271.01869.306.1871.0269.306.18
2189677-18967771.25371.25
3162529-16252961.05561.05
4194845-19484573.19473.19
5187655-18765570.49370.49
6183112-18311268.78768.79
10min1194532-19453273.07771.673.9173.2071.793.91
2193062-19306272.52472.64
3177560-17756066.70166.80
4199430-19943074.91775.04
5192030-19203072.13772.25
6188142-18814270.67670.79
15min1194742-19474273.15672.654.6073.4072.894.60
2194167-19416772.94073.18
3176850-17685066.43466.65
4199761-19976175.04175.29
5192618-19261872.35872.60
6202232-20223275.96976.20
20min1195422-19542273.41172.163.5773.7772.523.58
2194502-19450273.06573.43
3179712-17971267.51067.83
4199760-19976075.04175.41
5193298-19329872.61372.97
6189908-18990871.34071.70
30min1196432-19643273.79072.353.7174.2772.823.72
2195815-19581573.55974.04
3179115-17911567.28567.72
4199227-19922774.84075.34
5193898-19389872.83973.32
6191061-19106171.77372.25
45min1196196-19619673.70272.573.4074.3173.163.40
2196866-19686673.95374.56
3181341-18134168.12168.67
4200049-20004975.14975.77
5193537-19353772.70373.30
6191042-19104271.76672.36
极限1197412-19741274.15973.452.9874.8974.162.99
2198573-19857374.59575.32
3185308-18530869.61270.27
4202154-20215475.94076.69
5196703-19670373.89274.61
6192929-19292972.47573.19
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