普瑞巴林口崩片项目信息
介质体积(ml)900取样体积(ml)0补液体积(ml)0
对照品批号101106-202003对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.4对照品水分(%)0对照品稀释倍数100
标示量(mg)150供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
116.991058441056481059791057821056101057730.15
217.081049271048701048980.04
单位质量响应值RSD%判断
6225.606141.570.97数据可信
供试品溶液-LW0477批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
2min157140-5714055.11359.383.9855.1159.383.99
263322-6332261.07661.08
362231-6223160.02460.02
464131-6413161.85661.86
561050-6105058.88558.88
661490-6149059.30959.31
5min190600-9060087.38792.753.0687.3992.753.06
297676-9767694.21294.21
396893-9689393.45793.46
499225-9922595.70695.71
596286-9628692.87192.87
696296-9629692.88192.88
10min1100076-10007696.52799.131.6696.5399.131.66
2103753-103753100.073100.07
3103216-10321699.55599.56
4105046-105046101.320101.32
5101816-10181698.20598.20
6102723-10272399.08099.08
15min1102853-10285399.20599.980.9299.2199.980.92
2104380-104380100.678100.68
3103818-103818100.136100.14
4105033-105033101.308101.31
5102543-10254398.90698.91
6103291-10329199.62899.63
30min1103786-103786100.105100.170.95100.11100.170.95
2104458-104458100.753100.75
3103597-10359799.92399.92
4105399-105399101.661101.66
5102550-10255098.91398.91
6103323-10332399.65899.66
普瑞巴林口崩片项目信息
介质体积(ml)900取样体积(ml)0补液体积(ml)0
对照品批号101106-202003对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.4对照品水分(%)0对照品稀释倍数100
标示量(mg)150供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
116.991052321052031050481049871055141051970.20
217.081051451052611052030.08
单位质量响应值RSD%判断
6191.706159.430.37数据可信
供试品溶液-LW0477批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
2min154433-5443352.56955.624.6952.5755.624.69
257095-5709555.13955.14
355326-5532653.43153.43
459431-5943157.39557.40
557511-5751155.54155.54
661790-6179059.67459.67
5min195548-9554892.27591.901.8692.2891.901.86
293909-9390990.69290.69
392750-9275089.57389.57
496770-9677093.45593.46
594576-9457691.33791.34
697408-9740894.07294.07
10min196254-9625492.95798.112.7892.9698.112.78
2102525-10252599.01399.01
3101320-10132097.85097.85
4104039-104039100.475100.48
5101759-10175998.27498.27
6103653-103653100.103100.10
15min1100275-10027596.84099.511.6896.8499.511.68
2103823-103823100.267100.27
3102340-10234098.83598.83
4105176-105176101.574101.57
5102485-10248598.97598.97
6104141-104141100.574100.57
30min1101110-10111097.64799.431.3297.6599.431.32
2103374-10337499.83399.83
3102071-10207198.57598.57
4104796-104796101.207101.21
5102416-10241698.90898.91
6103992-103992100.430100.43
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