替米沙坦氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100374-202106对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数10000
标示量(mg)5供试品稀释倍数10系数0.7211
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.792703327122268282715227013270300.47
213.862720227110271560.24
单位质量响应值RSD%判断
1960.121959.310.03数据可信
供试品溶液-2026031821批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min115186-1518655.82353.8514.7055.8253.8514.70
215580-1558057.27157.27
316155-1615559.38559.38
410355-1035538.06438.06
514852-1485254.59554.60
615768-1576857.96257.96
10min119650-1965072.23269.974.9072.7970.514.90
217474-1747464.23364.81
320024-2002473.60774.20
418453-1845367.83268.21
519129-1912970.31770.86
619482-1948271.61572.19
15min121246-2124678.09975.892.5679.3877.132.55
220425-2042575.08176.30
321025-2102577.28778.62
420449-2044975.16976.23
520929-2092976.93478.18
619796-1979672.76974.06
20min121989-2198980.83078.592.1982.8980.592.12
221239-2123978.07380.04
321451-2145178.85380.96
421757-2175779.97881.79
521186-2118677.87979.90
620659-2065975.94177.96
30min121993-2199380.84578.233.5783.7181.013.39
221092-2109277.53380.28
320882-2088276.76179.65
422438-2243882.48185.09
520752-2075276.28379.08
620531-2053175.47178.25
45min122370-2237082.23176.366.0585.9179.925.80
220365-2036574.86178.38
320947-2094777.00080.66
422028-2202880.97484.41
519203-1920370.58974.15
619721-1972172.49376.03
60min121571-2157179.29474.776.4783.7979.106.16
220708-2070876.12180.39
320287-2028774.57479.00
421849-2184980.31684.56
518969-1896969.72973.99
618660-1866068.59372.86
极限120908-2090876.85774.295.0582.1579.374.86
220571-2057175.61880.65
321526-2152679.12884.30
420106-2010673.90978.96
519422-1942271.39476.36
618724-1872468.82873.78
替米沙坦氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100374-202106对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数10000
标示量(mg)5供试品稀释倍数10系数0.7211
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.792665826720268762674026655267300.34
213.862665926544266020.31
单位质量响应值RSD%判断
1938.361919.340.70数据可信
供试品溶液-2026031821批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min115194-1519456.74753.8715.0856.7553.8815.08
210735-1073540.09440.09
313270-1327049.56149.56
415282-1528257.07657.08
514991-1499155.98955.99
617077-1707763.78063.78
10min119104-1910471.35171.814.5871.9272.354.63
218743-1874370.00270.40
318117-1811767.66468.16
419505-1950572.84873.42
519146-1914671.50772.07
620744-2074477.47678.11
15min121151-2115178.99677.134.8080.2878.394.80
220822-2082277.76778.87
319135-1913571.46672.64
421041-2104178.58579.88
519862-1986274.18275.46
621895-2189581.77583.19
20min120350-2035076.00480.085.4778.0882.115.40
222715-2271584.83786.72
320008-2000874.72776.61
421715-2171581.10283.19
521080-2108078.73180.75
622784-2278485.09587.33
30min121182-2118279.11279.865.5581.9482.695.48
222540-2254084.18486.91
319992-1999274.66777.30
421636-2163680.80783.70
520126-2012675.16877.97
622824-2282485.24488.33
45min121942-2194281.95080.754.3085.5784.384.25
222783-2278385.09188.66
320268-2026875.69879.08
421137-2113778.94482.65
521189-2118979.13882.69
622401-2240183.66487.60
60min121433-2143380.04979.765.0484.4984.204.98
222470-2247083.92288.34
319913-1991374.37278.51
421191-2119179.14583.64
520482-2048276.49780.84
622645-2264584.57689.35
极限120231-2023175.56075.624.5680.8080.854.46
220843-2084377.84683.10
318598-1859869.46174.34
421327-2132779.65384.94
520147-2014775.24680.36
620331-2033175.93381.55
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