替米沙坦左氨氯地平片项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号100629-202204对照品来源中检院对照品使用方法直接使用
对照品含量(%)100.0对照品水分(%)0对照品稀释倍数1250
标示量(mg)80供试品稀释倍数10系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.137531707542637533567528557537657534820.08
211.167523297526827525060.04
单位质量响应值RSD%判断
67698.2967428.850.29数据可信
供试品溶液-2024070321批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1208856-20885627.82127.606.8727.8227.606.88
2208631-20863127.79127.79
3233813-23381331.14631.15
4195803-19580326.08326.08
5197648-19764826.32826.33
6198436-19843626.43326.43
10min1378881-37888150.47052.286.7450.6252.436.74
2417642-41764255.63355.79
3431432-43143257.47057.64
4367520-36752048.95749.10
5390030-39003051.95552.10
6369371-36937149.20349.35
15min1584907-58490777.91573.385.9578.3573.825.94
2567518-56751875.59876.06
3585117-58511777.94378.43
4520128-52012869.28569.70
5536631-53663171.48471.92
6510748-51074868.03668.46
20min1658029-65802987.65586.017.3088.5286.867.28
2643806-64380685.76086.64
3720041-72004195.91696.84
4615335-61533581.96882.77
5657322-65732287.56188.39
6579673-57967377.21778.02
30min1700093-70009393.25896.412.4894.6197.742.38
2717487-71748795.57596.94
3712007-71200794.84596.30
4749750-74975099.873101.13
5725807-72580796.68498.00
6737221-73722198.20499.43
45min1705650-70565093.99997.712.7095.8799.572.64
2712385-71238594.89696.79
3750464-75046499.968101.95
4745377-74537799.290101.10
5736319-73631998.08499.94
6750795-750795100.012101.78
60min1717635-71763595.59598.213.4797.99100.613.40
2706808-70680894.15396.57
3752588-752588100.251102.79
4732536-73253697.58099.94
5778324-778324103.679106.08
6735569-73556997.984100.31
极限1711411-71141194.76698.113.0797.69101.073.04
2717621-71762195.59398.53
3775932-775932103.361106.46
4738604-73860498.388101.29
5739034-73903498.446101.42
6736693-73669398.134101.01
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