盐酸伐地那非片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号D23106010771对照品来源中检所对照品使用方法直接使用
对照品含量(%)90.12对照品水分(%)0对照品稀释倍数1000
标示量(mg)10供试品稀释倍数1系数0.9306
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
1 12.073748203749133748933752543744463748650.08
2 12.143745193750423747800.10
单位质量响应值RSD%判断
31057.5830871.500.43数据可信
供试品溶液-BXJVV51批-pH1.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1390988-39098895.30891.494.7695.3191.494.76
2386581-38658194.23494.23
3387421-38742194.43994.44
4380916-38091692.85392.85
5358075-35807587.28587.29
6347976-34797684.82384.82
10min1404121-40412198.50997.083.0698.6797.243.06
2408911-40891199.67799.83
3399606-39960697.40997.57
4410212-41021299.994100.15
5385281-38528193.91794.06
6381538-38153893.00493.15
15min1403936-40393698.46497.342.2298.7997.662.23
2411153-411153100.223100.55
3401234-40123497.80698.13
4401899-40189997.96898.29
5389421-38942194.92695.23
6388270-38827094.64594.94
20min1403890-40389098.45397.612.0598.9498.082.05
2411955-411955100.419100.91
3400991-40099197.74698.23
4403716-40371698.41198.90
5391098-39109895.33595.80
6390864-39086495.27895.73
30min1403970-40397098.47397.681.8099.1298.321.81
2411152-411152100.223100.88
3400618-40061897.65598.30
4403136-40313698.26998.92
5390996-39099695.31095.93
6394452-39445296.15296.77
45min1403460-40346098.34897.591.7999.1698.401.79
2411701-411701100.357101.18
3399226-39922697.31698.12
4401670-40167097.91298.72
5391078-39107895.33096.11
6395075-39507596.30497.08
60min1403446-40344698.34597.551.7199.3298.521.72
2410884-410884100.158101.15
3400467-40046797.61998.59
4400475-40047597.62198.60
5391643-39164395.46896.40
6394305-39430596.11797.05
极限1401438-40143897.85597.772.5799.0098.902.56
2420339-420339102.463103.62
3398725-39872597.19498.33
4400413-40041397.60598.74
5390184-39018495.11296.21
6395397-39539796.38397.48
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