诺氟沙星胶囊项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号130450-201907对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.6对照品水分(%)0对照品稀释倍数100
标示量(mg)100 供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.054080084408148940804044079298408231140807170.03
210.064018208401690940175580.03
单位质量响应值RSD%判断
406041.49399359.641.18数据可信
供试品溶液-25021批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1479387-47938710.67211.248.5610.6711.248.55
2555865-55586512.37412.37
3562079-56207912.51312.51
4492655-49265510.96710.97
5458195-45819510.20010.20
6482654-48265410.74410.74
10min11350708-135070830.06831.023.2830.0931.043.28
21465794-146579432.63032.65
31428566-142856631.80231.82
41392223-139222330.99331.01
51366186-136618630.41330.43
61356078-135607830.18830.21
15min12225662-222566249.54649.001.4149.6149.071.42
22229198-222919849.62549.70
32228173-222817349.60249.68
42188098-218809848.71048.78
52177753-217775348.47948.55
62156939-215693948.01648.08
20min12876933-287693364.04463.480.9464.1963.640.95
22855740-285574063.57263.73
32867580-286758063.83663.99
42853608-285360863.52563.68
52856489-285648963.58963.74
62800211-280021162.33662.48
30min13725723-372572382.93982.540.6183.2082.800.61
23696714-369671482.29382.56
33682905-368290581.98682.25
43743851-374385183.34383.60
53704124-370412482.45882.71
63694504-369450482.24482.50
45min14259437-425943794.82094.771.4495.2295.161.43
24187807-418780793.22693.63
34197460-419746093.44193.84
44354844-435484496.94497.34
54257237-425723794.77195.16
64286077-428607795.41395.80
60min14374309-437430997.37897.601.5597.9398.161.55
24314789-431478996.05396.61
34308452-430845295.91296.47
44468679-446867999.478100.04
54382909-438290997.56998.12
64457017-445701799.21999.77
极限14377540-437754097.45098.041.8298.1798.761.81
24306424-430642495.86696.58
34333665-433366596.47397.19
44506593-4506593100.322101.05
54419640-441964098.38799.10
64480698-448069899.746100.46
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