褪黑素颗粒项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号520023-202203对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数10000
标示量(mg)1供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
1 9.856533965326654226542365356653730.08
2 9.896519365097651450.11
单位质量响应值RSD%判断
6636.856586.960.54数据可信
供试品溶液-2025041121批-pH1.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min172145-7214598.10696.731.3498.1196.731.34
271769-7176997.59497.59
372034-7203497.95597.95
470433-7043395.77895.78
570083-7008395.30295.30
670327-7032795.63395.63
10min172009-7200997.92197.601.2598.0897.761.25
272527-7252798.62598.79
373025-7302599.30299.47
471252-7125296.89197.05
570753-7075396.21396.37
671064-7106496.63696.80
15min171486-7148697.20997.112.0897.5497.442.08
273227-7322799.57799.90
372395-7239598.44698.77
471489-7148997.21497.53
571056-7105696.62596.94
668838-6883893.60993.93
20min171921-7192197.80197.721.4098.2998.211.40
272748-7274898.92699.42
373303-7330399.680100.17
470756-7075696.21796.70
570949-7094996.47996.96
671494-7149497.22097.70
30min172147-7214798.10897.781.0998.7698.421.10
272714-7271498.87999.54
372853-7285399.06899.73
471115-7111596.70597.35
571103-7110396.68997.33
671481-7148197.20397.84
极限172213-7221398.19897.711.3399.0198.521.33
272561-7256198.67199.49
372966-7296699.222100.05
471430-7143097.13397.94
570286-7028695.57896.38
671661-7166197.44798.25
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