玛巴洛沙韦片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号DQTL-4125-250109对照品来源工作对照品对照品使用方法直接使用
对照品含量(%)99.77对照品水分(%)0对照品稀释倍数2500
标示量(mg)20供试品稀释倍数5系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.331022871020001017831015641011681017600.42
211.341012101004161008130.56
单位质量响应值RSD%判断
8981.478890.040.73数据可信
供试品溶液-2025051521批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min125612-2561225.73725.927.7125.7425.927.71
223846-2384623.96323.96
327481-2748127.61627.62
427332-2733227.46627.47
527505-2750527.64027.64
623007-2300723.12023.12
10min136237-3623736.41536.813.5036.7037.103.53
235371-3537135.54435.81
337702-3770237.88738.19
437212-3721237.39437.70
538220-3822038.40738.71
635060-3506035.23235.49
15min140138-4013840.33541.032.7241.0341.732.75
239314-3931439.50740.17
342482-4248242.69043.42
441178-4117841.38042.10
541449-4144941.65242.39
640432-4043240.63041.28
20min143824-4382444.03943.541.3745.1844.701.41
242636-4263642.84543.95
343724-4372443.93845.14
443972-4397244.18745.37
543131-4313143.34244.54
642686-4268642.89543.99
30min146192-4619246.41845.842.0548.0547.482.05
244055-4405544.27145.85
345793-4579346.01747.71
446826-4682647.05548.73
545465-4546545.68847.37
645348-4534845.57047.15
45min147266-4726647.49848.161.1749.6450.311.17
248032-4803248.26750.34
348698-4869848.93751.14
448431-4843148.66850.86
547482-4748247.71549.90
647665-4766547.89949.98
60min148269-4826948.50648.891.0851.1851.571.13
247953-4795348.18850.79
349241-4924149.48252.23
448771-4877149.01051.74
549220-4922049.46152.18
648446-4844648.68351.30
90min147709-4770947.94349.691.8251.1552.911.71
250139-5013950.38553.52
349796-4979650.04053.34
449920-4992050.16553.44
549283-4928349.52452.79
649831-4983150.07553.23
120min150413-5041350.66051.531.3254.4055.311.27
250899-5089951.14854.85
352087-5208752.34256.19
450837-5083751.08654.92
551466-5146651.71855.53
651990-5199052.24555.96
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
极限151777-5177752.03151.141.0656.3455.491.00
250084-5008450.32954.60
350905-5090551.15455.59
450805-5080551.05455.46
550874-5087451.12355.51
650875-5087551.12455.42
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