盐酸氟西汀胶囊项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100513-202203对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数1000
标示量(mg)20供试品稀释倍数2系数0.8946
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.484875064878194879494874204879984877380.06
211.544887724867924877820.29
单位质量响应值RSD%判断
42485.8942268.800.37数据可信
供试品溶液-JS1M批-水
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1245914-24591446.62945.969.0046.6345.969.00
2202088-20208838.31938.32
3255844-25584448.51248.51
4265734-26573450.38750.39
5239652-23965245.44145.44
6245224-24522446.49846.50
10min1499429-49942994.69991.932.3595.2292.442.33
2481013-48101391.20791.63
3472900-47290089.66990.21
4473213-47321389.72890.29
5485723-48572392.10092.60
6496619-49661994.16694.68
15min1493838-49383893.63991.762.3195.2193.292.27
2488556-48855692.63794.08
3483765-48376591.72993.26
4463439-46343987.87589.43
5481253-48125391.25292.78
6492587-49258793.40294.96
20min1487137-48713792.36892.561.0994.9895.111.04
2493541-49354193.58296.05
3478252-47825290.68393.24
4488936-48893692.70995.24
5490643-49064393.03395.58
6490313-49031392.97095.57
30min1491566-49156693.20892.551.9596.8496.131.89
2492856-49285693.45396.96
3469702-46970289.06292.62
4486692-48669292.28495.85
5495740-49574093.99997.58
6492097-49209793.30996.94
极限1491202-49120293.13991.434.5697.8196.044.37
2495369-49536993.92998.48
3437911-43791183.03487.59
4486753-48675392.29596.88
5487775-48777592.48997.11
6494150-49415093.69898.37
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